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81.
Two analytical methods have been evaluated for quantitative determination of de-conjugated chrysene metabolites in fish bile. High performance liquid chromatography-fluorescence (HPLC-F) and gas chromatography-mass spectrometry (GC--MS) were compared regarding instrumental and overall limits of detection (LOD) as well as recoveries for the following nine chrysene compounds: 1-, 2,- 3-, 4- and 6-hydroxychrysene (1-, 2-, 3-, 4- and 6-OH-chr), 1,2-dihydroxy-1,2-dihydrochrysene (1,2-DHD-chr), 3,4-dihydroxy-3,4-dihydrochrysene (3,4-DHD-chr), 5,6-dihydroxy-5,6-dihydrochrysene (5,6-DHD-chr) and chrysene. Instrumental LODs were comparable for the two methods whereas the overall LOD was better for HPLC-F. Recoveries varied per chrysene compound for both HPLC-F (62-107%) and GC-MS (48-124%). In vivo formed chrysene metabolites were studied in the bile of Atlantic cod (Gadus morhua) exposed to chrysene (1 mg/kg) via intra-peritoneal (i.p.) and inter-muscular (i.m.) injection. Total amounts of chrysene metabolites were three times higher in i.p. compared to i.m. exposed cod bile, but the relative distribution of determined metabolites was very similar. 1,2-DHD-chr was the most prominent metabolite in de-conjugated bile and constituted more than 88% of the total chrysene metabolites. Additional chrysene metabolites formed were 3,4-DHD-chr and 1-, 2-, 3- and 4-OH-chr. K-region chrysene metabolites (oxidation at carbons 5 and 6) were not detected and seem to be a less favoured biotransformation route. The two methods were applied and evaluated for analysis of chrysene metabolites in two bile reference materials (BCR 720 and 721) and a limited number of field exposed cods. 相似文献
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Sugimoto JD Labrique AB Ahmad S Rashid M Shamim AA Ullah B Klemm RD Christian P West KP 《Disasters》2011,35(2):329-345
The epidemiology of tornado-related disasters in the developing world is poorly understood. An August 2005 post-tornado cohort study in rural Bangladesh identified elevated levels of death and injury among the elderly (≥ 60 years of age) (adjusted odds ratio (AOR) = 8.9 (95 per cent confidence interval (CI): 3.9-20.2) and AOR = 1.6 (95 per cent CI: 1.4-1.8), respectively), as compared to 15-24 year-olds, and among those outdoors versus indoors during the tornado (AOR = 10.4 (95 per cent CI: 5.5-19.9) and AOR = 6.6 (95 per cent CI: 5.8-7.5), respectively). Females were 1.24 times (95 per cent CI: 1.15-1.33) more likely to be injured than males. Elevated risk of injury was significantly associated with structural damage to the house and tin construction materials. Seeking treatment was protective against death among the injured, odds ratio = 0.08 (95 per cent CI: 0.03-0.21). Further research is needed to develop injury prevention strategies and to address disparities in risk between age groups and between men and women. 相似文献
85.
Simon P. Boilard Paul R. Amyotte Faisal I. Khan Ashok G. Dastidar Rolf K. Eckhoff 《Journal of Loss Prevention in the Process Industries》2013,26(6):1646-1654
Explosibility of micron- and nano-titanium was determined and compared according to explosion severity and likelihood using standard dust explosion equipment. ASTM methods were followed using a Siwek 20-L explosion chamber, MIKE 3 apparatus and BAM oven. The explosibility parameters investigated for both size ranges of titanium include explosion severity (maximum explosion pressure (Pmax) and size-normalized maximum rate of pressure rise (KSt)) and explosion likelihood (minimum explosible concentration (MEC), minimum ignition energy (MIE) and minimum ignition temperature (MIT)). Titanium particle sizes were ?100 mesh (<150 μm), ?325 mesh (<45 μm), ≤20 μm, 150 nm, 60–80 nm, and 40–60 nm. The results show a significant increase in explosion severity as the particle size decreases from ?100 mesh with an apparent plateau being reached at ?325 mesh and ≤20 μm. Micron-size explosion severity could not be compared with that for nano-titanium due to pre-ignition of the nano-powder in the 20-L chamber. The likelihood of an explosion increases significantly as the particle size decreases into the nano range. Nano-titanium is very sensitive and can self-ignite under the appropriate conditions. The explosive properties of the nano-titanium can be suppressed by adding nano-titanium dioxide to the dust mixture. Safety precautions and procedures for the nano-titanium are also discussed. 相似文献
86.
Rossella Guerrieri Rolf Siegwolf Francesco Ripullone Marco Borghetti 《Environmental pollution (Barking, Essex : 1987)》2010,158(9):2841-2847
We investigated the effect of N deposition (Ndep) on intrinsic water-use efficiency (WUEi), the ratio of photosynthesis (A) to stomatal conductance (gs), for two Quercus cerris stands at different distances to an oil refinery in Southern Italy. We used δ13C in tree rings for assessing changes in WUEi; while the influence of climate and NOx emission was explored through δ18O and δ15N, respectively. Differences in WUEi between the two sites were significant, with trees exposed to different degrees of NOx emissions showing an abrupt increase with the onset of pollution. Assuming similar gs at the two sites, as inferred through δ18O, the higher N availability at the polluted site caused the shift of the A/gs ratio in favour of A. Overall, our result suggests that an increase of Ndep may enhance tree WUE under a scenario of reduction of precipitation predicted for Mediterranean area. 相似文献
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EU Directive 91/414/EEC describes the authorization procedure for plant protection products. According to annex VI of this directive, the EU member states have to ensure that a plant protection product does not have unacceptable effects on the environment. The data requirements and the function of laboratory and field tests in the assessment procedure are discussed for the terrestrial compartment. 相似文献
89.
人们正加大努力以求最大限度地降低杀虫剂的使用,这些杀虫剂是控制茶树和其它作物的病虫害的基本手段 .在中国,由于土壤常常缺少碳酸钾,所以适量使用这种养料有助于减少对杀虫剂的需要 .已经证实,在土壤中加入钾后,茶树感染真菌病的比率下降 . 相似文献
90.
John?A.?VucetichEmail author Leah?M.?Vucetich Rolf?O.?Peterson 《Behavioral ecology and sociobiology》2012,66(2):295-303
For a wide range of taxa, partial prey consumption (PPC) is a frequent occurrence. PPC may arise from physiological constraints
to gut capacity or digestive rate. Alternatively, PPC may represent an optimal foraging strategy. Assessments that clearly
distinguish between these causes are rare and have been conducted only for invertebrate species that are ambush predators
with extra-intestinal digestion (e.g., wolf spiders). We present the first strong test for the cause of PPC in a cursorial
vertebrate predator with intestinal digestion: wolves (Canis lupus) feeding on moose (Alces alces). Previous theoretical assessments indicate that if PPC represents an optimal foraging strategy and is not caused by physiological
limitations, then mean carcass utilization is negatively correlated with mean kill rate and the utilization of individual
carcasses is uncorrelated with time between kills. Wolves exhibit exactly this pattern. We explore how the typical portrayal
of PPC by wolves has been not only misleading but also detrimental to conservation by promoting negative attitudes toward
wolves. 相似文献