炸药废水中TNR含量直接光度法测定的研究

以三硝基间苯二酚 ( TNR)溶于水后 ,溶液呈现出明显的亮黄色 ,据此直接用光度法对炸药废水中 TNR的含量进行了测定 ,并论证了光度法的测试条件。同时以消解测氮法进行印证 ,结果表明方法具有可行性     

两种吹扫捕集浓缩仪在测定土壤VOCs时的性能比较

从仪器精密度、方法检出限、准确度等角度对吹扫捕集浓缩仪Stratum PTC与Eclipse 4660的性能进行比较。结果表明,大部分分析物用Stratum PTC的方法检出限略高于Eclipse 4660,但精密度比Eclipse 4660稍差;Eclipse 4660用于分析极性的、水溶性物质的效果比Stratum PTC好,回收率更高。两种吹扫捕集仪的测试结果均满足《土壤和沉积物挥发性有机物的测定吹扫捕集/气相色谱-质谱法》(HJ 605-2011)标准方法的指标要求。     

基于PSO-SVM算法的环境监测数据异常检测和缺失补全

针对环境监测数据异常和数据缺失问题,提出了基于支持向量机的粒子群优化数据异常检测和缺失补全算法。利用粒子群优化算法选取较优的支持向量机训练参数组合,以此建立非线性的支持向量机模型,并利用结果模型对测得的真实数据拟合预测。以宁夏回族自治区某污水处理厂的污染物测量数据作为实验数据,结果表明,利用该算法预测数据的准确率可达97.977%,检测异常数据准确度高,缺失数据补全正确。     

容检规中非圆形缺陷可接受准则的安全裕度

文章以国内典型压力容器用材245R为例，采用GB／T19624~断裂力学评价方法对于《压力容器定期检验规程》表5、表6中的超标非圆形缺陷可接受准则的安全裕度进行评价，评价结果表明其中可接受准则的部分规定不够保守，就此作者给出相关的修改建议。     

CONFLICTING PERSPECTWES ABOUT DETECTION LIMITS AND ABOUT THE CENSORING OF ENVIRONMENTAL DATA1

ABSTRACT: Current conventions for reporting analytical results from environmental samples brings the objectives of laboratory scientists into conflict with those of environmental scientists. The objective of chemical analyses is to provide estimates of the true composition of samples. Reported results must reflect the analytical uncertainty. Current conventions require left-censoring of those results below the Limit of Detection. The objective of statistical interpretation of environmental data is to provide estimates of the characteristics of ecosystems. Such statistical analyses are often confounded by left-censoring of analytical results. We review the different points of view and propose a compromise which recognizes these conflicting perspectives.     

A TAU-LIKE TEST FOR TREND IN THE PRESENCE OF MULTIPLE CENSORING POINTS1

ABSTRACT: A common problem arises in testing for trends in water quality when observations are reported as “less than detection limit.” If a single detection limit is used for the entire study, existing non-parametric statistical methods, modified for ties, are applicable. If, however, the detection limit varies during the course of the study, resulting in multiple detection limits, then the commonly used trend detection methods are not appropriate. A statistic similar to Kendall's tau, but based on expected ranks, is proposed. Monte Carlo simulations show that the normal approximation to the distribution of this statistic is quite good, even for small samples and a large proportion of censored observations. The statistic is also shown to have greater power than the ad-hoc method of treating all observations less than the target censored observation as tied.     

大空间室内火灾早期自动探测与定位研究

本文在深入研究早期火灾一般燃烧火焰在彩色影像上所呈现的光谱及运动特性基础上，首次提出利用彩色影像实时探测室内火灾的新方法，通过物方坐标与像方坐标的直接线性变换，实现了早期火灾的自动探测与空间定位，实验证明了该方法的有效性与稳健性，且具有巨大的应用前景。     

Use of chemical cues in detection of conspecific predators and prey by newts, <Emphasis Type="Italic">Notophthalmus viridescens</Emphasis>

Summary. Detection of heterospecific predators and prey via chemical cues is well known, but only a few studies have examined the potential for such discrimination in cannibalistic systems. In newts, Notophthalmus viridescens, adults are opportunistic predators of conspecific larvae. I used a laboratory bioassay to determine whether larvae and adults distinguish between chemical stimuli from members of the different age classes. Larvae distinguished between chemical stimuli from larvae and adults by decreasing their activity only following exposure to stimuli from adults. Decreased activity is consistent with an antipredator response in many prey species, including larval newts. In contrast, adults increased their activity and increased time spent in open areas in response to stimuli from larvae, but not to stimuli from adults. Increased activity is consistent with a feeding response; adults also showed increased activity and increased time in open areas in response to chemical stimuli from familiar heterospecific prey (brine shrimp). The proximate cue that allowed the newts to distinguish between the different age classes is not associated with short-term dietary differences because all stimulus animals were fed the same prey. Stimulus strength was controlled by diluting the stimulus solutions according to the volume of the stimulus animal. Therefore, there appear to be intrinsic differences in the chemical signatures of larval and adult newts.     

管道泄漏检测技术

管道运输作为一种经济、有效、环保的运输方式,在液体、气体运输中具有独特的优势,管道泄漏检测是管道运输安全运行的关键和重要保障.通过总结国内外管道泄漏检测的最新方法,按运输对象分类介绍了管道运输气体和液体时的检测方法和工作原理,分析其优缺点,提出管道运输泄漏检测的对策,为提高我国管道运输的安全生产管理水平做出有益的探讨.