对Ag—DDC光度法测砷的分析

用Ａｇ－ＤＤＣ光度法测砷时，影响测定结果的准确度因素较多．本文重点阐述影响原因及其解决办法．     

厚壁管变形横波周向超声检测工艺及缺陷定位系统开发

在理论研究的基础上，利用试块对厚壁管变型横波与折射横波检测灵敏度进行了比较，证实了变型横波在厚壁管件中的检测灵敏度高于折射横波；设计开发计算软件，实现缺陷进行自动定位，大大提高现场检测效率和定位精度。     

涡流检波器建模研究及参数识别

笔者分析了涡流检波器的工作原理 :综合考虑了检波器磁路系统中 ,外壳、磁靴等部件的电磁感应对固定线圈感应电流的影响 ;建立了七参数的动力学模型。理论分析表明 :涡流检波器的外壳系统的附加耦合效应 ,影响了检波器的频率特性。在上述分析和研究的基础上 ,设计了检波器参数识别实验系统 ;验证了七参数动力学模型的合理性 ;研究的结论为检波器结构设计中改善和控制其特性参数、提高其工作安全可靠性等 ,提供了理论依据。     

Drink driving deterrents and self-reported offending behaviours among a sample of Queensland motorists

Problem

The efficacy of drink driving (driving under the influence, DUI) countermeasures to deter motorists from driving over the legal limit is extremely important when considering the personal and economic impact the offending behavior has on the community. This paper reports on an examination of 780 Queensland motorists' perceptions of legal and non-legal sanctions and their deterrent impact on self-reported offending behavior. Method: The data were collected via a telephone survey of motorists recruited from a random sample of all listed telephone numbers in the state, adjusted according to district population figures. Results: The results indicated that there were a range of legal and non-legal factors that were significantly associated with self-reported DUI including: the perceived risk of apprehension and license loss (legal factors); and concerns relating to the possibility of being involved in a crash and hurting another person (non-legal factors). However, additional multivariate analyses indicated that while both legal and non-legal factors significantly predicted self-reported DUI, higher alcohol consumption levels and more favorable attitudes to the behavior also appear to increase the likelihood of DUI. Discussion: The paper will outline the direct implications of the research project such as the development and promotion of countermeasures that both effectively deter motorists and address pro-offending attitudes. Impact on industry: The findings also highlight that DUI remains a relatively common behaviour among some motoring groups and that there is a need to extend current levels of enforcement as well as adopt innovative strategies to enhance the impact of these operations on the offending behaviour.     

Integrated testing and intelligent assessment—new challenges under REACH

BACKGROUND, AIM AND SCOPE: Due to a number of drawbacks associated with the previous regime for the assessment of new and existing chemicals, the European Union established a new regulation concerning the registration, evaluation, authorisation and restriction of chemicals (REACH). All relevant industrial chemicals must now be assessed. Instead of the authorities, industry itself is responsible for the risk assessment. To achieve better and more efficient assessments while reducing animal testing, all information-standard, non-standard and non-testing-has to be used in an integrated manner. To meet these challenges, the current technical guidance documents for risk assessment of new and existing chemicals had to be updated and extended considerably. This was done by experts in a number of REACH Implementation Projects. This paper presents the most relevant results of the expert Endpoint Working Group on Aquatic Toxicity in order to illustrate the change of paradigm in the future assessment of hazards to the aquatic environment by chemical substances. MAIN FEATURES AND CHALLENGES: REACH sets certain minimum data requirements in order to achieve a high level of protection for human health and the environment. It encourages the assessor to use alternative information instead of or in addition to standard one. This information has to be equivalent to the standard information requirement and adequate to draw overall conclusions with respect to the regulatory endpoints classification and labelling, persistent, bioaccumulative and toxic (PBT) assessment and predicted no-effect concentrations (PNEC) derivation. The main task of the expert working group was to develop guidance on how to evaluate the toxicity of a substance based on integration of information from different sources and of various degrees of uncertainty in a weight of evidence approach. INTEGRATED TESTING AND INTELLIGENT ASSESSMENT: In order to verify the equivalence and adequacy of different types of information, a flexible sequence of steps was proposed, covering characterisation of the substance, analysis of modes of action, identification of possible analogues, evaluation of existing in vivo and in vitro testing data as well as of QSAR results. Finally, all available data from the different steps have to be integrated to come to an overall conclusion on the toxicity of the substance. This weight of evidence approach is the basis for the development of integrated testing strategies (ITS), in that the available evidence can help to determine subsequent testing steps and is essential for an optimal assessment. Its flexibility helps to meet the different requirements for drawing conclusions on the endpoints classification and labelling, PNEC derivation as well as PBT assessment. The integration of all kinds of additional information in a multi-criteria assessment reduces the uncertainties involved with extrapolation to the ecosystem level. The weight of evidence approach is illustrated by practical examples. CONCLUSIONS AND PERSPECTIVES: REACH leads to higher challenges in order to make sound decisions with fewer resources, i.e. to move away from extensive standard testing to an intelligent substance-tailored approach. Expert judgement and integrated thinking are key elements of the weight of evidence concept and ITS, potentially leading to better risk assessments. Important sub-lethal effects such as endocrine disruption, which are not covered by the current procedure, can be considered. Conclusions have to be fully substantiated: Risk communication will be an important aspect of future assessments.     

Properties of Distillers Grains Composites: A Preliminary Investigation

Interest in renewable biofuel sources has intensified in recent years, leading to greatly increased production of ethanol and its primary coproduct, Distillers Dried Grain with Solubles (DDGS). Consequently, the development of new outlets for DDGS has become crucial to maintaining the economic viability of the industry. In light of these developments, this preliminary study aimed to determine the suitability of DDGS for use as a biofiller in low-cost composites that could be produced by rapid prototyping applications. The effects of DDGS content, particle size, curing temperature, and compression on resulting properties, such as flexural strength, modulus of elasticity, water activity, and color were evaluated for two adhesive bases. The composites formed with phenolic resin glue were found to be greatly superior to glue in terms of mechanical strength and durability: resin-based composites had maximum fiber stresses of 150–380 kPa, while glue composites had values between 6 kPa and 35 kPa; additionally, glue composites experienced relatively rapid microbial growth. In the resin composites, both decreased particle size and increased compression resulted in increased mechanical strength, while a moderate DDGS content was found to increase flexural strength but decrease Young’s modulus. These results indicate that DDGS has the potential to be used in resin glue-based composites to both improve flexural strength and improve potential biodegradability.     

Factorial structure of recklessness: to what extent are older drivers different?

PROBLEM: This study tests whether the original factorial structure of a recklessness questionnaire can be maintained for the current Spanish population of older drivers. JUSTIFICATION: Our recent interest in dedicating special attention to senior citizen mobility (Monterde, 2001), is due to the impending increase of the aging population in Western countries; this has led us to reinitiate the psychometric study of the construct validity, revising and including older drivers in the psychometric aspects of those evaluation instruments that will then be used in the Spanish psycho-medical check of drivers and in research. METHODS: Factorial analysis was used to determine validity. RESULTS: There was an appearance of a different psychological pattern in elderly drivers, specifically, a psychological anxiety trait related to the task of driving. Furthermore, interesting data were found about the attitude of this sector toward the "traffic society" and toward some of the measures included in Spanish legislation that affect especially older drivers (such as the psycho-medical check). IMPACT ON INDUSTRY, RESEARCH AND PRACTICE: These results suggest the possible existence of some kind of "compensation phenomenon," which could have influence over the scores obtained and their interpretation. Consequently, the evaluation instruments should be tested and, if necessary, adapted or specifically created for use with this age group.     

Utilization of waste foundry sand (WFS) in concrete manufacturing

Due to ever increasing quantities of waste materials and industrial by-products, solid waste management is the prime concern in the world. Scarcity of land-filling space and because of its ever increasing cost, recycling and utilization of industrial by-products and waste materials has become an attractive proposition to disposal. There are several types of industrial by-products and waste materials. The utilization of such materials in concrete not only makes it economical, but also helps in reducing disposal concerns. One such industrial by-product is waste foundry sand (SFS). Waste foundry sand is a by-product of ferrous and nonferrous metal casting industries. Foundries successfully recycle and reuse the sand many times in a foundry. When the sand can no longer be reused in the foundry, it is removed from the foundry and is termed as waste foundry sand.Published literature has shown that WFS could be used in manufacturing Controlled Low-Strength Materials (CLSM) and concrete. This paper presents an overview of some of the research published on the use of WFS in concrete. Effect of WFS on concrete properties such as compressive strength, splitting tensile strength, modulus of elasticity, freezing-thawing resistance, and shrinkage are presented.     

钢结构栓接板面抗滑移系数试验新法

此文详细介绍了一种钢结构栓接板面抗滑移系数试验的新方法,该方法简便、实用.     

典型飞机结构加速腐蚀试验方法研究

针对典型飞机结构的局部腐蚀环境开展了加速腐蚀环境谱及加速腐蚀试验方法研究,采用A和B两种加速腐蚀环境谱进行了对比试验。结果表明,在飞机结构加速腐蚀环境谱中采用铜加速乙酸盐雾试验,不仅具有明显的加速腐蚀作用,使试验历程大大缩短,而且能够较好地再现典型飞机结构的腐蚀损伤特征。