阳极溶出伏安法测定ppb级Cu,pb,Cd的实验条件的选择

本文介绍了在环境监测中，经试验研究，确定的用阳极溶出伏安法，连续分析环境样品中重金属Ｃｕ，Ｐｂ，Ｃｄ的最佳条件，即用悬汞电极做工作电极，用０．１Ｍ离氯酸做支持电解质，纯氮除氧。当ＰＨ值取２－７，富集电位数－１．１～－１．２Ｖ时，不但可连续测定一定浓度范围的重金属Ｃｄ，Ｐｂ，ＣＵ；而且方法灵敏度高，精密良好，线性相关关系可达０．９９９０，回收率达８５－１１５％，获得了良好的分析效果。     

氰化钠生产中聚合废料的利用

对氰化钠生产中的聚合废料进行了吸附试验和氰化钠含量分析，试验结果表明，聚合废料中含有２８％左右的氰化钠，其中黑褐色杂质可用活性炭吸附脱除。生产规模试验证明，用聚合废料为原料生产的硫氰酸钠，产品质量可达到装置设计指标，满足腈纶装置的使用要求。     

The basic properties of poly(lactic acid) produced by the direct condensation polymerization of lactic acid

Poly(lactic acids) with high molecular weights have been synthesized by direct condensation polymerization of lactic acid. These polymers have good mechanical properties and can be processed into products such as cups, film, and fiber, which can be used as compostable materials. This polymerization method can be applied to the synthesis of copolymers of lactic acid and other hydroxyacids. The properties of poly(lactic acid) and copolymers synthesized by the direct process are different from those of polymers obtained by the conventional lactide process.     

应用SSIM模型反演与评估二氧化硫污染面源

针对在缺少有效二氧化硫低空面源排放清单的情况下,应用SSIM(SourceStrengthInversedModel)模式对SO2低空面源源强的反演功能,完成了天津市蓝天工程改燃措施实施后二氧化硫相对量化改善效果的模拟评估,同时模拟了SO2面源源强改善前后的空间分布,取得了较理想的效果。该模式所解决的污染面源源强核查难点问题,在城市大气环境容量核定中具有通用指导作用。     

Viability analysis of management frameworks for fisheries

The pressure on marine renewable resources has rapidly increased over past decades. The resulting scarcity has led to a variety of different control and surveillance instruments. Often they have not improved the current situation, mainly due to institutional failure and intrinsic uncertainties about the state of stocks. This contribution presents an assessment of different management schemes with respect to predefined constraints by utilizing viability theory. Our analysis is based on a bio-economic model which is examined as a dynamic control system in continuous time. Feasible development paths are discussed in detail. It is shown that participatory management may lead to serious problems if a purely resource-based management strategy is employed. The analysis suggests that a less risky management strategy can be implemented if limited data are available.     

液膜分离在造纸黑液治理中的应用

液膜分离在造纸黑液治理中的应用潘碌亭朱亦仁（阜阳师范学院化学系，阜阳２３６０３２）吴成康（阜阳师范学院科技处）关键词液膜法；黑液；木质素．１前言目前，我国造纸工业普遍采用碱法制浆，而蒸煮制浆过程中产生的黑液含有大量的有机物和无机物，ＣＯＤ值很高，黑液...     

含油污水乳化液微波分离实验研究

针对油气田乳化含油污水难分离的特点,利用微波技术进行的实验室研究结果表明,微波辐照温度与其后的静置时间都是影响其破乳率的重要因素,其分离效果随微波辐照后温度的增高而加强,而且在相同温度下乳液破乳率随静置时间加长而迅速增高。研究结果证实,微波辐射技术具有时间短、能耗少、效率高等特点,且经过微波处理后的含油污水易于进行油品回收再利用,有良好的应用前景。     

废旧压敏胶粘标签清洗剂的研究

针对公共环境和商品上废旧残损压敏胶粘标签的清除，研制了2种压敏胶粘标签的水基清洗剂，进行了配方组分筛选试验，单因素试验及正交试验，优化出了分别含酯类溶剂和烃类溶剂的2类配方，通过添加适量的阴离子和非离子复配型表面活性剂，同时在适当的投料顺序，搅拌速度和时间，温度等工艺参数条件下，制备了均匀稳定的2类水基清洗剂，该清洗剂适于多种基材表面的压敏胶粘标签的清洗，具有对基材无腐蚀，环境污染小，低成本和常温使用等特点。     

Biosynthesis and Characterization of Laccase Catalyzed Poly(Catechol)

Enzymatic polymerization of catechol was conducted batch-wise using laccase enzyme produced by the culture Trametes versicolor (ATCC 200801). The polymerization reaction was carried out in 1:1 (v/v) aqueous-acetone solution, buffered at pH 5.0 with sodium acetate (50 mM) in a sealed, temperature-controlled reactor at 25°C. The molecular weight of the produced polymer was determined with GPC. FT-IR, DSC, and TGA were employed to investigate the structure and thermal behavior of synthesized poly(catechol). It was found that catechol units were linked together with ether bonds and thermal stability of the catechol increased in the poly(catechol) polymeric structure effectively. The number average molecular weight of poly(catechol) was found as 813 ± 3 Da with a very narrow polydispersity value of 1.17 showing selective polymerization of catechol by the enzyme.     

冷轧厂废水处理破乳系统的改造

叙述了冷轧厂废水处理破乳系统原设计存在的问题，全面地介绍了该系统改造方案的选择，确定及实施情况，重点说明了超滤破乳工艺流程，主要性能参数及改造后的效果。