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水相催化芳香氯化物脱氯研究 总被引:4,自引:0,他引:4
通过把起相转移作用的聚乙二醇(PEG)链,键合到硅胶上,再将聚乙烯吡咯烷酮(PVP)络合双金属Pd-Cu后负载其上,制成一种新型双负载双金属催化剂PVP-PdCl2/SiO2-PEG600,以甲酸钠为氢转移试剂,在水相催水芳香氯化物脱氯,当反应温度80℃左右,n(Pd):n(Cu)=2:1,反应介质pH值11.7左右时,具有较高的催化脱卤活性,催化剂不但易于制备,便于分离,且具有良好的重复使用性能,经重复使用六次,转化率仍在70%以上。 相似文献
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本方法是用固相萃取法萃取水和废水中的多菌灵,取浓缩纯化后的有机相直接进样到高效液相色谱仪,用二极管矩阵检测器检测,根据保留时间外标法定量. 相似文献
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In the conceptualization of thriving at work, it is emphasized that employees' learning and vitality are two equally important components of thriving and that thriving is facilitated by contextual features and available resources. In this study, we examined the effects of two challenge stressors (time pressure and learning demands) on thriving at work. Based on the literature on challenge and hindrance stressors, we proposed that challenge stressors positively affect learning and negatively affect vitality. To uncover underlying mechanisms, we measured challenge appraisal and hindrance appraisal of work situations in a diary study. A sample of 124 knowledge workers responded to three daily surveys (before the lunch break, during the afternoon, and at the end of the workday) for a period of five workdays. Results indicate that the indirect effects of learning demands and time pressure on learning are mediated by challenge appraisal, whereas indirect effects of learning demands on vitality are mediated by hindrance appraisal. Overall, our study shows that challenge stressors have a positive total effect on learning but no total effect on vitality. These differential relationships call for a finer distinction between the two components of thriving at work in future research. Copyright © 2016 The Authors Journal of Organizational Behavior Published by John Wiley & Sons Ltd. 相似文献
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The incessant demand and consumption of energy services among individuals’ is increasing throughout the world. Individuals’ electricity consumption in Northern Cyprus has risen considerably. However, the demand for electrical energy services on the island is heavily reliant on imported fossil fuels. Burning fossil fuels has adverse effects on its environment. Therefore, sustainable energy consumption is required and individuals are targeted for energy conservation to reduce electricity consumption. Against this background, using the Structural Equation Modeling approach, this research incorporates social‐psychological factors; personal norms, positive and negative emotions into the theory of planned behaviour (TPB) model to assess the relationships among the variables, explain their impact on consumers’ electricity conservation intentions and enhance the explanatory power of the model. Data was conveniently obtained from a quantitative sample of 400 electricity consumers. The results indicate that negative emotions have the strongest significant influence on intentions, but personal norms have the least effect on intentions to save electricity. Furthermore, the study revealed that our expanded TPB model can provide improved explanatory power more than the original TPB. Policy implications, limitations and future research are discussed. 相似文献
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Erhan Kayabasi Munip Alpaslan Alperen Hüseyin Kurt 《International Journal of Green Energy》2019,16(2):200-210
In this study, the effects of geometric properties such as baffle spacing, baffle cut, sealing strips, gaps between heat exchanger components, number of tubes and tube passes have been investigated for shell and tube heat exchangers (STHE). For this purpose, geometrical dimensions and data of a specific heat exchanger (HE) used in an industrial application have been obtained. The HTRI Xchanger Suite Educational software was utilized to analyze the reference HE, to verify the results of the software and the output temperatures of the fluids, the shell side heat transfer coefficient (HTC) and the pressure loss (PL) values were compared with the experimental data. After confirming that the results of the software were within the acceptable deviation values, the geometric dimensions of the reference design were changed and new analyzes were carried out to examine the effects of several dimension options on the performance of STHE. Results were discussed in a detailed and comprehensive manner via curves. 相似文献