"南海贻贝观察":广东沿海牡蛎体中Zn含量水平及其变化趋势

为了了解广东沿海重要养殖水域Zn含量水平变化趋势,1989～1997年间实施"南海贻贝观察"计划对广东12个地点牡蛎体的Zn含量进行了连续监测.广东沿海牡蛎体Zn含量范围为50.4×10-6～768×10-6,总平均值为245×10-6,总体上属清洁～微污染水平.牡蛎体Zn含量的海域分布格局呈珠江口海区＞粤东海区≥粤西海区.1989～1991年,广东沿海牡蛎体Zn含量呈上升趋势,此后略微下降,1994～1997年间牡蛎体Zn含量虽有波动,但年际间没有明显差异.     

工业用防锈铝合金板材的超塑性能研究

此文主要对工业牌号防锈铝合金板LF3、LF21进行了组织超塑性研究.结果表明,LF3防锈铝合金,在变形温度为470～510℃、ε_0=(5.56～11.1)×10~(-4)s~(-1)的试验条件下可实现超塑性;LF21防锈铝合金,在变形温度为510～540℃、ε_0=(5.56～8.83)×10~(-4)s~(-1)的试验条件下具有超塑性.     

外加锌在土壤中形态的研究

本文采用化学逐级提取法对吸附锌后的土壤分别提取了交换态、CaCO_3结合态、氧化物结合态和有机质结合态的锌量,并讨论pH、温度和溶液中锌离子浓度对不同形态锌分布的影响。实验结果表明:外加锌被石灰性土壤吸附后,高pH值(7.5)时形态分布为:CaCO_3结合态≥交换态>氧化物结合态>有机质结合态;低pH值(5.5)时则为:交换态>CaCO_3结合态>氧化物结合态>有机质结合态。各形态锌的分配系数还受到吸附时的温度和溶液中锌离子浓度的影响。     

Microstructure and mechanical properties of alloy C-276 weldments fabricated by continuous and pulsed current gas tungsten arc welding techniques

Effects of switching over from gas tungsten arc welding (GTAW) to pulsed current gas tungsten arc welding (PCGTAW) on the quality of joints produced in Hastelloy C-276 material were investigated. Welding was carried out both by autogenous mode and using ERNiCrMo-3 filler wire. Microstructures of weld joints produced with and without current pulsing were studied using optical and scanning electron microscopy. Microsegregation occurring in GTAW and PCGTAW joints was investigated using energy dispersive X-ray spectroscopy (EDS). Strength and ductility of weld joints produced with and without pulsing were evaluated. The results show that pulsing results in refined microstructure, reduced microsegregation and improved strength of weld joints. Secondary phase(s) noticed in GTA weldments were found to be absent in PCGTA weldments. Autogenous PCGTA weldments were found to be the best in terms of: (i) freedom from microsegregation, (ii) strength and (iii) freedom from unwanted secondary phases.     

基于SEM图像处理法的化学镀Ni-P合金表面改性基底层孔隙表征

目的对Ni-P合金表面层孔隙进行定量表征。方法通过SEM微观形貌图像分析孔隙分布,运用ImageJ软件对SEM图像进行处理,并统计分析Ni-P合金表面层孔隙的孔隙率、孔隙数目、等效直径等数据。结果电化学蚀刻在改性Ni-P合金表面层制备微孔层,随时间延长,表面微孔数量增多、孔径增大。蚀刻1,3,5 min的孔隙率分别为0.85%,4.34%,11.18%,蚀刻5 min后微孔发生交联,Ni-P合金层防护性能被破坏。结论电化学蚀刻3 min可在Ni-P合金表面层获得分布均匀、等效直径主要分布在100~850 nm之间的微孔。     

Effect of CO2 corrosion behavior of mild steel in oilfield produced water

The corrosion rates of API X65 mild steel alloy in CO₂ – containing produced water have been studied by weight loss technique, potentiodynamic polarization technique and characterization of the corroded surface techniques. The effect of temperature, speed of rotation, pH and acetic acid concentration were studied. The optimum condition in presence and absence of protective film were also addressed. The kinetic parameters and reaction behavior were discussed in details. Corrosion rates increases with increasing temperature, acetic acid concentration, and speed of rotation, and decreased with increasing solution pH. The primary corrosion product of API X65 mild steel is ferrous carbonate (FeCO₃) at high temperatures, high pH's (alkaline media) and absence of acetic acid, which could act as a protective film so that CO₂ corrosion rate can be reduced.     

提高大型锌合金成形模具精度并降低成本的工艺措施

结合制模工艺实践,提出并分析了提高大型锌合金模具精度并降低成本的一些工艺因素,介绍了设计方案和工艺措施,并对实际效果进行了讨论.     

铁磁形状记忆合金研究进展与展望(Ⅰ):材料、力学特性

综述了铁磁形状记忆合金(Ferromagnetic Shape Memory Alloy,简写为FSMA)在材料研制和热磁力学特性方面的研究现状,对其存在的问题进行了分析并指出其发展方向.在材料研发方面,介绍了新型合金、Ni-Mn-Ga-X系列合金、复合材料和Ni2MnGa系列合金;在热磁力学特性方面,介绍了形状记忆效...     

铝合金镀镍废水治理中存在问题及解决措施

本文针对铝合金镀镍废水处理中存在的主要问题进行了讨论,同时结合工作实践,从电镀废水水质特征、处理工艺及其可靠性进行了分析,并提出了一系列适用于国家新颁布的《电镀污染物排放标准》(GB21900-2008)的工艺措施。