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81.
Xiaolan Chai Jinping Jia Tonghua Sun Yalin Wang Liyan Liao 《Journal of environmental science and health. Part. B》2013,48(6):629-634
A novel and simple analytical procedure using cold activated carbon fiber-solid phase microextraction (CACF-SPME) was applied to determine organochlorine pesticides (OCs) in soil samples. The pesticides in this study consist of α -, β -, γ -, and δ -hexachlorocyclohexane (HCH). By heating the sample while cooling the fiber, the developed method not only provides better performance in terms of sensitivity, linearity and recovery but also offers shorter adsorption procedure than that of traditional headspace-solid phase microextraction (HS-SPME). The experimental conditions such as the amount of water, adsorption time and adsorption temperature were optimized. Matrix effects were investigated with different types of soils. We concluded that using the standard addition method was required for quantification purposes. The limits of detection obtained using the proposed method range from 0.01 to 0.05 ng/g, and the recoveries for CACF-SPME are in the range of 80.01% to 89.68% with relative standard deviation (RSDs) better than 8.60%. The proposed method was further applied to determine OCs in real agricultural soil. The results are in good agreement with those obtained using traditional ultrasonic extraction. The research demonstrates the suitability of the CACF-SPME for the analysis of OCs in soil. 相似文献
82.
Bin Cui Chongjun Zhang Liang Fu Dandan Zhou Mingxin Huo 《Frontiers of Environmental Science & Engineering》2023,17(6):73
83.
84.
低温环境对作业人员的影响及评价 总被引:3,自引:0,他引:3
低温环境在许多行业中都存在,它能影响作业人员的工作效率,甚至危害其身体健康,是劳动保护和劳动安全不可忽视的一个方面。本文主要从工程及生理学角度介绍不同的低温环境对作业人员的影响及相应的生理学反应;讨论对低温环境影响的评价方法及其应用,为低温环境作业人员的劳动保护及劳动安全提供一定的生理学依据。 相似文献
85.
冷原子荧光测定痕量汞影响空白值的因素 总被引:3,自引:0,他引:3
吕森伟 《环境监测管理与技术》1997,9(3):42-43
阐述了冷原子荧光法测定痕量汞影响空白值的诸因数,提出了消除方法。 相似文献
86.
我们通过对YYG-2型冷原子测汞仪荧光室和相应气路系统的改进,克服了原仪器在操作过程中汞蒸汽直接排于工作台面的现象,提高了仪器的稳定性能和灵敏度,减少了操作步骤和节省了载气,在不同程度上还减化了原仪器结构。通过实践证明改进后的仪器基本上满足了环境监测或其它测试分析的要求。 相似文献
87.
自行车变速轴零件的冷挤压是我国早期应用无屑加工技术制造高难度复杂零件的典型范例之一,此文作者针对4种内齿、内棘齿零件冷挤压成形的研制过程,着重介绍了其中一种零件的挤压工艺分析、实际生产工序和所用模具的特点,对长期处于保密状态的技术予以适当解密。 相似文献
88.
本研究以湖南省林业技术推广总站在湖南选育的17个耐寒桉树优良单株为试验材料,进行组培繁殖,有14个优良单株成功地诱导出了愈伤组织或芽。结果表明,以一年生扦插苗的当年生嫩枝作为外植体来源,污染率低且愈伤组织和芽的诱导率高;0.25%氯化汞消毒15—20分钟,可将污染率控制在70%以下,且对外植体的损害最小;按树最佳的诱导培养基为:1/2MS+BA_(1.0)+IBA_(0.25),最佳的继代培基为:MS+BA_(1.0)+KT_(1.0)+VB2_(10)。 相似文献
89.
用自制的冷原子汞蒸气发生装置和样品吸收管,研究了以SnCl_2为还原剂,冷原子吸收分光光度法连续测定汞的适宜条件.检出限为0.45ng/ml,汞量在0~80ng/ml范围内,符合比尔定律;连续测定浓度为20ng/m的汞溶液,相对标准偏差为1.8%;测定实际水样中的痕量汞,其回收率为97.0%~100.8%. 相似文献
90.
Kathrin Baumann Harald Maurer Gabriele Rau Martin Piringer Ulrike Pechinger Andr Prvt Markus Furger Bruno Neininger Umberto Pellegrini 《Atmospheric environment (Oxford, England : 1994)》2001,35(36):897
During the Mesoscale Alpine Programme (MAP) special observation period (SOP) between 7 September and 15 November 1999, ground-based and airborne measurements have been conducted in the Rhine valley south of the Lake of Constance to investigate the unstationary aspects of Foehn and related phenomena, like the impact of Foehn on the ozone concentrations in the valley. Foehn events occurred with above-average frequency and high diversity. Foehn induced ozone peaks in October and November are found to be much lower than the September Foehn case of the period. An inversion layer in the lake area with ozone concentrations below 10 ppb often shields the monitoring stations from the Foehn air aloft. Trajectory calculations for the Foehn period between 19 and 24 October 1999 reveal that the Foehn air originated from below 1 to 1.5 km above the Po Basin and the Mediterranean Sea. Tethered balloon soundings in the source area south of the Alps, ozone measurements at the mountain station Jungfraujoch (3580 m a.s.l.) and airborne measurements across the Alpine crests reveal that the ozone levels found in the Foehn air correspond to the concentrations just above the mixing height in the Po Basin and are transported across the Alpine crest within the lowest flow layer. 相似文献