全文获取类型
收费全文 | 3367篇 |
免费 | 201篇 |
国内免费 | 663篇 |
专业分类
安全科学 | 189篇 |
废物处理 | 111篇 |
环保管理 | 336篇 |
综合类 | 1819篇 |
基础理论 | 434篇 |
污染及防治 | 655篇 |
评价与监测 | 626篇 |
社会与环境 | 49篇 |
灾害及防治 | 12篇 |
出版年
2024年 | 16篇 |
2023年 | 57篇 |
2022年 | 78篇 |
2021年 | 106篇 |
2020年 | 124篇 |
2019年 | 101篇 |
2018年 | 82篇 |
2017年 | 108篇 |
2016年 | 148篇 |
2015年 | 155篇 |
2014年 | 198篇 |
2013年 | 293篇 |
2012年 | 259篇 |
2011年 | 334篇 |
2010年 | 168篇 |
2009年 | 184篇 |
2008年 | 167篇 |
2007年 | 191篇 |
2006年 | 177篇 |
2005年 | 116篇 |
2004年 | 109篇 |
2003年 | 149篇 |
2002年 | 107篇 |
2001年 | 105篇 |
2000年 | 97篇 |
1999年 | 63篇 |
1998年 | 99篇 |
1997年 | 68篇 |
1996年 | 57篇 |
1995年 | 45篇 |
1994年 | 44篇 |
1993年 | 41篇 |
1992年 | 43篇 |
1991年 | 14篇 |
1990年 | 14篇 |
1989年 | 13篇 |
1988年 | 12篇 |
1987年 | 12篇 |
1986年 | 14篇 |
1985年 | 4篇 |
1984年 | 17篇 |
1983年 | 11篇 |
1982年 | 14篇 |
1981年 | 12篇 |
1974年 | 2篇 |
1973年 | 1篇 |
1971年 | 1篇 |
1970年 | 1篇 |
排序方式: 共有4231条查询结果,搜索用时 171 毫秒
61.
饮用水中五种有机磷农药的快速检测法 总被引:6,自引:0,他引:6
本文介绍了使用Waters OASIS-HLB固相萃取小柱从水中分离富集敌百虫、敌敌畏、乐果、甲基对硫磷,对硫磷五种有机磷农药的快速检测法。 相似文献
62.
含硫化合物的气相色谱检测响应特性研究 总被引:4,自引:0,他引:4
利用气相色谱(配炎焰光度检测器)对二硫化碳(CS2)、甲硫醇(CH3CH)、甲硫醚(DMS)和二甲二硫醚(DMDS)4种含硫物质进行了分析检测,着重讨论了气相色谱仪的各项参数对几种含硫物质响应和分离效果的影响。结果表明:该分析对含硫气体的最小检测浓度达到ppb级。在各项参数中,色谱柱温度在N2压力对各含硫物质响应和分离度影响最大,汽化室和检测器温度及空气压力对它们的影响相对较小。 相似文献
63.
论述了高效液相色谱法适于环境样品中分子量大、挥发性低、热稳定性差的有机污染物的分析与分离。参阅了国内外文献,例举了用高效液相色谱法测定环境样品中多环芳烃、酚类、多氯联苯、酞酸酯类、联苯胺类、阴离子和非离子表面活性剂、有机农药等有机污染物的测定条件及分离结果。 相似文献
64.
Accurate diagnosis of mosaicism in amniotic fluid cell cultures represents a major problem. If insufficient cells are analysed, true fetal mosaicism may go undetected. False-positive diagnosis is also possible since a second cell line may arise in vitro and not reflect the true fetal genetic constitution. These difficulties apply to both flask and in situ culture techniques, to varying degrees. The relative accuracy of flask versus in situ culture techniques in excluding mosaicism was determined by statistical analysis of experimental data from ten pairs of mixed male-female amniotic fluid specimens. The data support the idea that the majority of in situ colonies are independent of one another. The following conclusions are drawn: (1) analysis of a single metaphase from a number of different colonies enhances the confidence for excluding mosaicism; (2) analysis of more than one cell per colony offers little advantage; (3) exclusion of a given level of mosaicism requires analysis of fewer metaphases using the in situ method; (4) the confidence for excluding mosaicism is high with both in situ and flask techniques, using the provided guidelines; and (5) it is shown that the two-stage approach used by many laboratories is currently the most efficient way to exclude mosaicism. 相似文献
65.
We describe our experience of prenatal diagnosis of non-ketotic hyperglycinaemia in four at-risk pregnancies using the glycine/serine ratio in amniotic fluid obtained between 18 and 20 weeks of gestation. All glycine levels were in the normal range. Serine levels were normal in two patients and borderline in the others. Glycine/serine ratios were normal in two patients, moderately increased in one patient ( + 3 SD), and highly increased in one patient ( + 8 SD). All the children were perfectly normal at birth. Because of this false-positive prediction and the false-negative prediction recently reported, we suggest that this unreliable method should not be used. 相似文献
66.
We report a gas chromatographic-mass spectrometric method which allows the very long chain fatty acids content of trophoblastic tissue to be directly measured in samples collected by biopsy between 8 and 11 weeks of gestation. This method has been successfully applied to the detection of fetal Zellweger syndrome in two pregnant women who had previously delivered affected infants. In one of them, increased concentrations of C26:0 (0.254 versus 0.108±0.035 μ/mg proteins) and C24:0 (1.32 versus 0.815±0.325 μ/mg proteins) in trophoblast indicated that the fetus had Zellweger syndrome, a diagnosis confirmed by pathological findings after abortion. In the second case, the pregnancy was allowed to proceed, on the basis of normal concentrations of very long chain fatty acids in trophoblastic tissue, and its outcome was actually a healthy newborn. 相似文献
67.
We studied the validity of mid-trimester amniotic fluid testosterone and FSH in the diagnosis of fetal sex in abnormal fetuses and in twins. It was found that the testosterone/FSH ratio, but not the level of the individual hormones, was an excellent criterion for fetal sex diagnosis. In a control group of 32 female and 34 male fetuses, the testosterone/FSH ratio was diagnostic. In two cases the values were indeterminate and fetal sex could not be predicted, but there were no false diagnoses. The abnormalities of the fetuses were diagnosed by karyotype analyses or raised levels of α-fetoprotein. It was found that neither autosomal trisomies nor X-chromosome aneuploidy or neural tube defect interfered with the diagnostic value of the hormonal approach. The twin study included 14 pairs, three of whom were discordant for sex. In all twins the fetal sex diagnosis was appropriate. In co-twins of the same sex the hormone levels were very close to each other. 相似文献
68.
We report relatively high citrulline concentration in amniotic fluid of a citrullinemic fetus suggesting that prenatal detection of this condition could be done on this basis in conjunction with a direct or an indirect determination of argininosuccinate synthetase activity in amniotic fluid cells. 相似文献
69.
David J. H. Brock 《黑龙江环境通报》1981,1(1):11-16
An analysis is made of alphafetoprotein (AFP) concentrations in 3630 amniotic fluids submitted for prospective prenatal diagnoses over a 7-year period. There were 89 cases of anencephaly, 74 of open spina bifida and 3467 with normal singleton outcomes. The AFP data were expressed in both standard deviations above the mean and multiples of the normal median for individual weeks of gestation. False positive and false negative rates were comparable in the two systems at selected cut-offs. It is concluded that either system may be used in setting action limits for the primary distinction of unaffected pregnancies from those in which an open neural tube defect is present. 相似文献
70.