超临界二氧化碳萃取－GC／MS测定土壤中的多环芳烃

本文开发了一种采用超临界二氧化碳萃取土壤中多环芳烃、不须经过纯化步骤，直接可用于ＧＣ／ＭＳ分析的简便、高效的方法。本实验中超临界革取的流体是二氧化碳，改善剂是５％的二氯甲烷／甲醇，萃取温度为１２０℃、压力为３４ＭＰａ。ＧＣ／ＭＳ分析时除了采用外标外，还加入了６种同位素ＰＡＨｓ内标以校正各段ＰＡＨｓ的响应因子。采用本方法成功地测定了我国未开垦森林土壤中的ＰＡＨｓ。     

苏州河氨化菌分布及生理生化研究

对苏州河氨化菌进行了生态调查,并对其进行了生理生化分析。研究结果表明,苏州河水体中氨化菌数量普遍较高,上游至下游氨化菌数量逐步增多。氨化菌数量与水体中总氮和氨氮呈正比,与硝酸盐成反比。     

离子色谱分析中的几个问题探讨

在掌握离子色谱技术最新发展动态的基础上,对离子色谱的新进展、前处理新技术、常用的改善分离度方法、若干注意事项、常遇到的问题等进行了分析探讨,以期用离子色谱技术更多更好地解决实际问题.     

固相微萃取-毛细管气相色谱法快速同步分析水中有机氯及有机磷农药

固相微萃取是一种快速、简便,集萃取浓缩进样于一体的样品前处理技术,具有分析时间短、灵敏度高、无需有机溶剂的优点.用固相微萃取富集水中8种有机氯及7种有机磷农药,毛细管气相色谱ECD检测器分离分析,整个分析过程只需26min,检出限可达0.002～1μg/L,已用于地表水中有机氯及有机磷农药含量的测定.     

螯合树脂在线富集——火焰原子吸收光度法测定水中微量Cu,Pb,Zn,Cd

对螯合树脂在线富集，火焰原子吸收光度法进行了条件试验。试验证实方法对Ｃｕ、Ｐｂ、Ｚｎ、Ｃｄ４个元素检出浓度可达μｇ／Ｌ级，校准曲线性、样品重现性及准确度可满足测定要求。     

科技论文的写作

本文介绍了科技论文的写作步骤和基本格式,指出科技论文写作中应注意的事项。     

近年来宁夏对沙尘天气的监测及对沙漠化防治对策

宁夏在全区范围内建立沙尘暴监测网络,开展对沙尘天气的应急监测。宁夏作为沙源区和沙尘过往的主要通道,2002年全区共监测沙尘天气12次,沙尘粒径多分布在大于2 1μm。为防治沙漠化,宁夏积极寻求国际间合作,采取退耕还林还草、划管封育、禁牧、把握人工降雨时机等一系列措施,加大对沙漠化的防治力度。     

肿瘤病房医用直线加速器对周围环境电离辐射的调查分析

通过对医院肿瘤病房医用直线加速器机房周围环境的电离辐射监测调查 ,并计算分析各相关人群的年有效剂量当量 ,结果低于《辐射防护规定》(GB870 3- 88)中的标准限值。表明医用直线加速器机房的辐射防护设施设计是安全合理的 ,具有重要的现实意义 ,该辐射防护设施具有推广价值。     

Desert Water Harvesting to Benefit Wildlife: A Simple, Cheap, And Durable Sub-Surface Water Harvester for Remote Locations

A sub-surface desert water harvester was constructed in the sagebrush steppe habitat of south-central Idaho, U.S.A. The desert water harvester utilizes a buried micro-catchment and three buried storage tanks to augment water for wildlife during the dry season. In this region, mean annual precipitation (MAP) ranges between about 150–250 mm (6″–10″), 70% of which falls during the cold season, November to May. Mid-summer through early autumn, June through October, is the dry portion of the year. During this period, the sub-surface water harvester provides supplemental water for wildlife for 30–90 days, depending upon the precipitation that year. The desert water harvester is constructed with commonly available, “over the counter” materials. The micro-catchment is made of a square-shaped, 20 mL. “PERMALON” polyethylene pond liner (approximately 22.9 m × 22.9 m = 523 m²) buried at a depth of about 60 cm. A PVC pipe connects the harvester with two storage tanks and a drinking trough. The total capacity of the water harvester is about 4777 L (1262 U.S. gallons) which includes three underground storage tanks, a trough and pipes. The drinking trough is refined with an access ramp for birds and small animals. The technology is simple, cheap, and durable and can be adapted to other uses, e.g. drip irrigation, short-term water for small livestock, poultry farming etc. The desert water harvester can be used to concentrate and collect water from precipitation and run-off in semi-arid and arid regions. Water harvested in such a relatively small area will not impact the ground water table but it should help to grow small areas of crops or vegetables to aid villagers in self-sufficiency.     

CTL-12型化学需氧量速测仪与标准法测定CODCr之比较

使用CTL—12型化学需氧量速测仪分析废水化学需氧量，简便、快速，且方法可行，完全能满足环境监测技术要求。