集安市世界遗产旅游发展现状及对策分析

高句丽王城、王陵和贵族墓葬世界文化遗产是已消失的高句丽文明的历史见证。该遗产地包括3座王城、14座王陵和26座贵族墓葬,其中除五女山城外,其他遗产均位于中国吉林省集安市境内。通过对集安遗产旅游发展的自身优势、机遇、问题进行综合分析,认为集安遗产旅游发展处于初级阶段,潜力巨大,并提出发展策略：确立旅游发展目标、加强城市营销,完善基础设施、提升交通网络通达性,拓宽融资渠道、构建文化遗产产业链及加强区域合作、协同发展。     

浅析氧化风机在电厂烟气脱硫工程中的应用

作为整个脱硫运行中比较关键的大型设备,氧化风机的选型是否合理,直接关系整个工程的投资及运营。本文从罗茨鼓风机和离心鼓风机各自的工作原理和特点分析了两种风机在实际脱硫工程中的优缺点,同时在风机效率、噪声大小及风机传动设施方面进行了比较说明。     

Residents＇ Attitudes Towards Tourism in a Globally Important Agricultural Heritage Systems Pilot Site： a Case Study in China

Globally Important Agricultural Heritage Systems （GIAHS） is a wide program to promote the conservation and adaptive management of such systems and their associated landscapes, biodiversity, knowledge systems and cultures. Rice-Fish Systems （RFS） in Longxian village of China, as a traditional agricultural system, was selected as one of the five pilot sites of GIAHS in 2005. Researchers have paid more attention to the dynamic conservation and adaptive management of RFS because it is under severe threats from global development challenges. Tourism is suggested to be brought into the RFS conservation program as an alternative industry. This paper presents a comparative study of residents in three types of farm household in Longxian, seeking attitudes to the RFS conservation and tourism development and ways in which such information may guide future strategies. Results show residents, belonging to the household type in which most family members are abroad, have the most positive attitudes to RFS conservation and tourism development; while residents, as other household type in which less than 50% of family members are abroad, are the least sensitive group in these three household types, due to the motivation of moving abroad weakening their enthusiasm to participate in the local activities. Implications are discussed in the context of how resident attitudes will affect the future management of GIAHS conservation and tourism development, and then measures are put forward to foster tourism cooperation and multistakeholders process establishment.     

微电解法预处理对氟硝基苯废水的研究

采用废铁屑微电解法对氟硝基苯废水进行预处理，在铁粉投加量为3.0g/L、phH为3．0、反应时间为3h、催化剂氯化铵用量为2.0g/L的条件下，对氟硝基苯转化为氨基氟苯的转化率为70％、出水的BOD5／COD值由0上升到0．27。     

琉基葡聚糖凝胶分离富集-二溴对甲偶氮羧微乳液分光光度法测定微量镍

研究了在溴代十六烷基吡啶（CPB）、正丁醇、正庚烷、水自制微乳溶液存在下,镍与二溴对甲偶氮羧（DBpMCA）的显色反应,在pH值为9．07的Na2B4O7-HCl缓冲溶液中,镍与试剂形成淡红色配合物,最大吸收峰位于560nm波长处,表观摩尔吸光系数ε为2．8×10^5L／（mol·cm）。优化了试验条件,考察了共存离子的影响,方法在0．002mg／L～0．320mg／L范围内符合比尔定律,检出限为0．0006mg／L,生活垃圾、水、土壤样品测定的RSD为2．1％～5．2％,加标回收率为96．6％～104％。     

M‐(p‐Nitrobenzyl) pyridine as a spray reagent for the thin‐layer chromatographic detection of dimethyl tetrachloroterphthalate herbicide

Abstract

The developed thin‐layer chromatogram of DCPA (Dacthal) is sprayed with 4‐(p‐nitrobenzyl)pyridine chromogenic reagent followed by ammonium carbonate solution. The chromatogram is then heated in an oven at 130°C for 20 minutes. When cool, the chromatogram is sprayed with tetraethylenepentamine reagent. DCPA spots appear blue against a white background. The sensitivity of this test is about 1 μg. The procedure is useful to detect DCPA in water and in soil.     

Laboratory studies on volatilization and mineralization of 14c‐p,p'‐DDT in soil,release of bound residues and dissipation from solid surfaces

Abstract

In support of field data, laboratory studies were conducted on volatilization, mineralization and binding of ¹⁴C‐p,p'‐DDT in soils at Sao Paulo. Incubation of soil for 6 weeks did not result in volatilized organics or mineralization; with >95% extractable radiocarbon in the form of p,p'‐DDT. Small amounts of bound residues (1.8%) were detected in soil. These data confirm the very slow dissipation of DDT in the field which presumably relates to the acidic pH of soil (4.5–4.8).

Bound ¹⁴C‐residues in soils treated with ¹⁴C‐p,p'‐DDT at Praia Grande and Sao Paulo could be released (5–21%) by sulphuric acid treatment. The released residue had the composition: 69–90% DDT, 7–32% DDD and 0–3% DDE. Incubation of soil bound ¹⁴C‐residues with fresh inoculum for 3 months did not result in release of ¹⁴C.

Dissipation from wooden surfaces was fairly slow. After 20 weeks, 74% of the applied radioactivity could be recovered; 44% hexane‐non‐extractable.     

树脂D001负载纳米Pd/Fe双金属脱溴2,2＇,4,4＇-四溴联苯醚（BDE-47）的研究

采用大孔树脂D001交换吸附Pd2＋、Fe2＋并在厌氧条件下以硼氢化钠溶液还原吸附的钯铁离子制备成负载纳米Pd/Fe双金属树脂。利用该树脂对2,2＇,4,4＇-四溴联苯醚（BDE-47）进行脱溴反应,探讨了该法的可行性和特性。结果表明：当大孔树脂D001、氯化钯、硫酸亚铁用量分别为0.75 g、2μg和0.2 g时所制备的双金属树脂脱溴水-乙醇溶液中的BDE-47效果最佳,反应遵循准一级动力学,速率常数k约为0.161 d-1,半减期为1.21 d。负载Pd/Fe的D001连续3次脱溴反应都有较好的效果,水-乙醇溶液中超过90%以上的BDE-47在反应6 d后被降解。负载Pd/Fe双金属的树脂可以重复活化再生,但再生2次后其脱溴效率变差,反应6 d只有47.3%的BDE-47被降解。用气相色谱-质谱联用仪和离子色谱仪跟踪Pd/Fe双金属树脂脱溴BDE-47反应,可知产物包括溴离子、三溴联苯醚、二溴联苯醚、一溴联苯醚和联苯醚。     

关于对氨基二甲基苯胺光度法测定硫化物方法的探讨

本文通过大量的实验证明对氨基二甲基苯胺光度法测定水中硫化物的吹气时间可由原来的25min缩短到10min,与原方法进行对照,其精密度和准确度符合要求。从而得出结论：将吹气时间原方法的25min缩短到10min,既节省了时间,又不影响方法的精密度和准确度。     

潞安矿区土地复垦模式研究

矿产资源的开采在给人类提供财富的同时,也给矿区带来了一系列的生态环境问题,尤其对土地的破坏极为严重,但通过合理的整治和复垦,破坏的土地可以得到恢复。针对潞安矿区的土地复垦进行初步探讨,在分析潞安矿区土地复垦现状的基础上,论述了潞安矿区复垦中存在的一系列问题及应采取的相应措施和方法。