原子吸收法测定水中镉的质量控制指标研究

通过全国多家实验室的大量监测数据,研究分析了镉测定的质量控制指标,并与《水质镉的测定双硫腙分光光度法》（GB/T 7471-1987）和《环境水质监测质量保证手册》（第二版）进行了比较,旨在为环境监测工作提供质量控制依据和质量控制指标。研究表明,标准样品的精密度质量控制指标范围：RSD≤5.0%和RSD’≤8.0%;准...     

民航事故征候的关联度分析和灰色模型预测

民航事故征候的分析和预测是民航安全研究的重要内容,其目的是掌握民航事故征候影响因素的影响程度和未来发展状况,以此提出相应的安全措施,减少民航事故.通过对民航事故征候及其影响因子作灰色关联度分析,发现机组失误是关键因子,其后依次为总飞行时间、机械原因和天气原因;运用灰色模型对现有2001-2004年机组失误导致的事故征候的实测统计数据进行分析,预测出2005-2009年机组失误导致的事故征候次数分别为37、44、52、61和73;经过残差、后验差等检验分析,发现该模型精度较高,效果较理想.预测的趋势指示出机组失误导致的事故征候随时间的推移在增加.所以,在以后的航空安全管理工作中要着重加强机组管理,有效的预防和矫正机组行为失误,从而达到减少事故征候的目的.     

碱性过硫酸钾法测定总氮的精密度偏性实验分析

通过碱性过硫酸钾法测定总氮的精密度偏性实验及其结果分析,提出测定总氮的过程中应注意功能室的环境要求及一些细小的分析细节,并提出相应的建议.     

基于性能退化数据分析的训练装备精度保持性评估

目的对训练装备的精度保持性评估问题进行专门研究。方法跟踪监测训练装备使用过程中精度的退化情况,并计算出每个监测时刻训练装备的综合精度指数,预测训练装备失效的寿命值。结果通过精度指数与时间的回归模型,分别得到装备的失效水平和所预测的失效寿命T',以此为基础评估训练装备的精度保持性。结论训练装备的精度保持性是用户关心的重要质量指标,对在训练装备使用过程中获取的成效有直接影响,精度保持性评估结果还是用户确定合理精度调整及训练装备大修周期的重要参考依据。     

测定化学需氧量的新型分光光度法

研究了一种测定化学需氧量(COD Mn)的新型分光光度法。试验结果表明,该法简便快速、准确,精密度高,并且通过与国标法测定结果对比后确定该方法可用于自来水、饮用水等多种水体中COD Mn的测定。     

An approach to uncertainty estimation in determining polycyclic aromatic hydrocarbons in fuel-contaminated soils

An estimation of uncertainty contribution in the entire set of the analytical data of polycyclic aromatic hydrocarbons (PAHs) in soil during a full year is presented. The analyses were performed as part of a project devoted to the assessment of the natural attenuation of selected PAHs in agricultural soil contaminated by a fuel spill. In particular, we investigated the effect of natural attenuation on the PAH dissipation rate in plots of two types of scenarios in agricultural soils. One of them was previously affected by an accidental fuel spill 10 years ago, and the other one was non-affected. The major components for estimating uncertainty contributions have been evaluated based on intermediate precision from different levels of PAH mass fraction, sample locations, and long term data set. An analysis of variance (ANOVA) test was applied to the mass fractions of clean or blank soil sub-samples versus contaminated soil sub-samples for grouping comparable data. Variables of influence in this study were site, month, and lysimeter of sampling (referring to a stainless steel box, with side lengths of 50 cm). Study sites or the spatial arrangement of lysimeter showed a clear effect in sub-sample results with the lowest mass fraction levels for heavier PAH, while monthly sampling was the variable of most significant influence for the more strongly contaminated sub-sample results.

Finally, the results of the PAH mass fractions in contaminated soil sub-samples indicated a monthly variation for which lighter, volatile PAHs rapidly decreased while the less volatile did not change.     

非稳定流巷道火灾试验系统的研制

介绍了巷道火灾试验系统的构成,测定燃烧区膨胀热阻时测点位置的确定方法,火灾时期烟气温度、壁温及岩体温度、烟流中CO2及O2体积分数、沿程压力和风速等的测试方法及测试仪表精度,系统抗干扰方法,数据采集和处理软件的功能以及测试系统的调试方法.系统采用无补偿导线经济地解决了巷道燃烧区测温热电偶冷端温度补偿的方法,使测温系统误差由过去的10%左右下降到3%.     

DISTRIBUTED RUNOFF FORMULATION DESIGNED FOR A PRECISION AGRICULTURAL LANDSCAPE MODELING SYSTEM1

A precision scale landscape model designed for agricultural applications is described in this paper. The Precision Agricultural Landscape Modeling System (PALMS) is a combination of two process‐based models: a diffusive wave runoff model with ponding (described in detail) and a biosphere model with a crops module (briefly reviewed). Several innovations, including numerical formulations for the hydrologic properties of the soil surface with crusting, slope/tillage angle interactions, and change of roughness and detention storage with cumulative precipitation have been included. The model is compared to observations on one 1.8 ha field planted with maize and soybeans during four growing seasons, and one 24 ha field planted with maize during one growing season. Daily average soil moisture is simulated well (within 5 percent volumetric), except in extended runoff/ponding episodes. Physical processes not simulated in the model suggest possible explanations for model errors. Planned improvements for PALMS are also presented.     

用通用有限元程序分析精密设备基础沉降的方法

采用弹性有限元方法计算了设备对地基的附加应力 ,根据土力试验数据验算了地基的沉降 ,完成了要用专门的土力学程序分析计算的工作 ,得到满意的结果。本文的工作对于精确分析基础沉降有借鉴作用。     

ESTIMATES OF MEAN CHLOROPHYLL-a CONCENTRATION: PRECISION,ACCURACY, AND SAMPLING DESIGN1

ABSTRACT: Data from 56 north-temperate lakes and reservoirs are used to develop models predicting temporal variance as a function of the mean chlorophyll-a concentration. Trophy, as estimated by mean chlorophyll-a concentration, is shown to have little effect on the sampling effort required to achieve a pre-determined level of precision for lakes sampled year-round. Collecting ten observations results in a coefficient of variation that averaged 20 percent; collecting more than ten observations yields increasingly marginal improvements in precision. The same guidelines apply to mesotrophic or eutrophic lakes sampled in the summer, whereas oligotrophic lakes sampled in the summer require fewer observations to achieve the same level of precision. The bias resulting from collecting too few observations is minimized if five or more observations are collected.