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71.
新型混凝剂聚硅硫酸铝的研究 总被引:15,自引:0,他引:15
以硫酸铝、水玻璃、铝酸钠为主要原料制备的新型混凝剂聚硅硫酸铝,其产品的Al2O3含量约8%,盐基度40% ̄60%,对制备的PASS溶液经5个月的贮存,其性质稳定,PASS在去浊试验中,无论常温和低温均低优于硫酸铝。对三种工业废水进行混凝处理,取得令人满意的CODcr去除率。 相似文献
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聚硅氯化铝混凝剂除油效果的试验 总被引:10,自引:0,他引:10
制备不同碱化度和不同Al/Si摩尔比的系列聚硅氯化铝作为混凝剂,实验考察了B,Al/Si摩尔比及PH值对除油效果的影响,并考察了PASC去除COD的效果。结果表明,B对PASC混凝除油效果影响较大,随B值增大,除油效果提高;Al/Si摩尔比对PASC混凝除油效果影响较小; 相似文献
73.
Yonghao Wang Wenqi Wei Yuzhi Lin Mian Zhang Yongjing Wang Minghua Liu 《环境科学学报(英文版)》2020,32(8):111-118
In this work, magnesium silicate-based sulfonated polystyrene sphere composites (SPS/MgSi) were synthesized by one-step (SMD1) and two-step (SMD2) methods. For SMD1, MgSi particles were densely assembled on the surface of SPS, assisted by complexation between Fe3+ and hydroxyl phenol. For SMD2, SPS/SiO2 was firstly obtained by the same method as SMD1, and then SPS/SiO2 was transformed directly to SPS/MgSi under hydrothermal conditions. Therefore, MgSi obtained by the two-step method had an interwoven structure. Compared to SPS, MgSi and SMD1, SMD2 presented a larger specific surface area and more negative surface charges. Therefore, SMD2 showed superior adsorption performance toward CIP with concentrations of 5, 10 and 50 mg/L, and for 50 mg/L, the equilibrium adsorption capacity could reach 329.7 mg/g. The adsorption process is fast and can be described by the pseudo-second-order kinetic model. The relationship between pH value and Zeta potential demonstrated that electrostatic interaction dominated the adsorption process. In addition, competitive adsorption showed that the effect of Na+ was negligible but the effect of Ca2+ was dependent on its concentration. Humid acid (HA) could slightly promote the absorption of CIP by SMD2. After five rounds of adsorption-desorption, the equilibrium adsorption capacity of SMD2 still remained at 288.6 mg/L for 50 mg/L CIP. Notably, SMD2 presented likewise superior adsorption capacity for CIP with concentrations of 10 and 50 mg/L in Minjiang source water. All the results indicated that this synthesis method is universal and that SMD2 has potential as an adsorbent for CIP removal from aquatic environments. 相似文献
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高效负载型光催化剂制备及其加铂修饰技术 总被引:7,自引:0,他引:7
通过光催化氧化五氯苯酚钠实验,结合对催化剂晶型结构、比表面积的表征分析,优化钛酸四丁酯水解制备TiO2负载型催化剂并加铂修饰的制备条件:R值、烧结温度、粘合剂添加量、空心玻璃珠粒径大小及催化剂中铂含量,从而制备出高效、实用的负载加铂修饰型半导体光催化剂.实验结果表明,当R=10,温度为650℃烧结1h,TiO2∶硅酸钠∶空心玻璃珠=10∶2.5∶20(W),铂在催化剂中的重量百分比为1.4%~1.6%,空心玻璃珠的粒径为0.5mm时,所制备的加铂修饰负载型催化剂催化活性、使用寿命和牢固度均比较理想.用该催化剂做光催化实验,当反应液初始五氯苯酚钠浓度为100mg/L、pH值为6.5,催化剂投加量为2g/L,通氧气量为1.6mL/s,光照强度为30kW/m2时,五氯苯酚钠2 h光催化氧化率达92.0%. 相似文献