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石墨炉原子吸收光谱法测定海河下游水中痕量镉 总被引:2,自引:0,他引:2
原子吸收光谱法直接测定高盐水中痕量镉时,有很大背景吸收和误差。本文采用络合—萃取技术使共存元素与待测元素分离,既消除了基体干扰,又达到了富集作用,使测定结果准确可靠。 相似文献
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湿法吸收测定大气中的五氧化二磷 总被引:1,自引:0,他引:1
用2%NaOH溶液吸收大气中的P2O5,用钼锑抗试剂显色定量。对样品的稳定性、方法的显色条件、精密度、准确度以及检出限进行反复试验,结果令人满意。 相似文献
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在线自动监测仪与实验室国标方法测定地表水中总氮的比对分析 总被引:2,自引:2,他引:2
随着监测技术的发展,地表水中越来越多的污染物可采用自动监测仪器实现实时监测。采用自动监测与实验室国标方法测定地表水中总氮的结果是否可比以及造成差异的原因,文章根据实际样品比对实验对此进行了探讨。 相似文献
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对螯合树脂在线富集,火焰原子吸收光度法进行了条件试验。试验证实方法对Cu、Pb、Zn、Cd4个元素检出浓度可达μg/L级,校准曲线性、样品重现性及准确度可满足测定要求。 相似文献
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采用火焰原子吸收分光光度法测定鱼内脏及河流底泥中的铜。鱼内脏经组织捣碎机捣成匀浆后,加硝酸消解;底泥则经氢氟酸和高氯酸消化。该方法具有灵敏度高,精密度和回收率较好等特点。 相似文献
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Using improved neural network model to analyze RSP,NOx and NO2 levels in urban air in Mong Kok,Hong Kong 总被引:4,自引:0,他引:4
As the health impact of air pollutants existing in ambient addresses much attention in recent years, forecasting of airpollutant parameters becomes an important and popular topic inenvironmental science. Airborne pollution is a serious, and willbe a major problem in Hong Kong within the next few years. InHong Kong, Respirable Suspended Particulate (RSP) and NitrogenOxides NOx and NO2 are major air pollutants due to thedominant diesel fuel usage by public transportation and heavyvehicles. Hence, the investigation and prediction of the influence and the tendency of these pollutants are ofsignificance to public and the city image. The multi-layerperceptron (MLP) neural network is regarded as a reliable andcost-effective method to achieve such tasks. The works presentedhere involve developing an improved neural network model, whichcombines the principal component analysis (PCA) technique and theradial basis function (RBF) network, and forecasting thepollutant levels and tendencies based in the recorded data. Inthe study, the PCA is firstly used to reduce and orthogonalizethe original input variables (data), these treated variables arethen used as new input vectors in RBF neural network modelestablished for forecasting the pollutant tendencies. Comparingwith the general neural network models, the proposed modelpossesses simpler network architecture, faster training speed,and more satisfactory predicting performance. This improvedmodel is evaluated by using hourly time series of RSP, NOx and NO2 concentrations collected at Mong Kok Roadside Gaseous Monitory Station in Hong Kong during the year 2000. By comparing the predicted RSP, NOx and NO2 concentrationswith the actual data of these pollutants recorded at the monitorystation, the effectiveness of the proposed model has been proven.Therefore, in authors' opinion, the model presented in the paper is a potential tool in forecasting air quality parameters and hasadvantages over the traditional neural network methods. 相似文献
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Goyal SK 《Environmental monitoring and assessment》2003,89(3):305-314
Sodium arsenite (modified Jacobs and Hochheiser method; hereafter referred as SA), the most widely used manual monitoring method for determination of nitrogen dioxide (NO2) in ambient air, particularly in developing countries has been evaluated and compared with US EPA recommended equivalent method of TGS-ANSA (hereafter referred as ANSA). NO2 concentrations generated from laboratory test atmosphere were analyzed by these two methods and were compared statistically. Laboratory evaluations showed that SA method has high sensitivity to different sampling conditions, which normally vary during actual field monitoring. Hence, correction factors for absorption efficiency were estimated for SA and ANSA methods. Absorption efficiency of NO2 in SA method was found to be much lower (64%) as against the reported value of 82% at the method recommended sampling conditions, whereas for ANSA method, it was found 1.0 as against the reported value of 0.93. After applying derived correction factors, both the methods produced almost similar concentration values of NO2. 相似文献
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