Direct hydride derivatization of methyl- and ethylmercury chlorides in aqueous solution with KBH4

A convenient hydride derivatization procedure of methyl-and ethylmercury chlorides to volatile hydrides was reported. In sealed vials methylmercury and ethylmercury compounds in acidic aqueous solutions were converted into their volatile forms by the reaction with potassium tetrahydroborate(KBH4) and elvolved to the headspace of the vials. The gaseous analytes in the headspace were extracted and concentrated by solid phase microextraction(SPME) and injected into gas chromatography (GC) for separation and identified by mass selective detector(MS).     

煤炭燃烧排砷水平与控制技术研究

煤炭是我国目前的主要一次能源之一,燃煤中的重金属污染愈来愈受到重视,如何控制煤炭中砷向环境中扩散,减轻环境污染是近年来重要的研究课题.通过开展对铁法煤业集团内部高砷煤和低砷煤的动力配煤燃烧试验,分析动力配煤燃烧过程中的砷迁移水平,研究铁法煤业集团内部动力配煤燃烧过程中的砷迁移规律和动力配煤降砷的可行性,并为开展最佳动力配煤操作数据提供理论依据,为高砷煤燃烧控制砷的排放寻找治理途径,提高煤炭资源的最大利用效率.     

环境和质量管理体系一体化实质分析

阐述了过程方法在ISO14001（2004版）环境管理体系标准和ISO9001（2000版）质量管理体系标准中的运用。介绍了过程的概念、过程特性的概念、过程的输入和输出要求。分析了环境管理体系和质量管理体系一体化的实质及其意义。指出一体化管理体系不是将2个标准中要素的要求简单叠加。     

精对苯二甲酸残渣的处理现状及综合利用

综述了国内外精对苯二甲酸（PTA）生产企业的残渣处理概况和残渣中有价物质的回收方法：提出了PTA残渣的控制和综合利用思路，分析了PTA残渣综合利用的经济效益。     

一种新型烟气除尘脱硫脱氮一体化装置

提出了一种新型高效烟气除尘脱硫脱氮一体化装置,该装置将三种先进的技术有机结合,取得了相得益彰的效果:采用独特溢流装置的自激式除尘器进行除尘和脱硫脱氮,采用球面筛板塔进行二次除尘和脱硫脱氮,采用结构新颖的汽水分离器进行进一步除尘和脱硫脱氮。该装置不仅实现烟气的高效脱硫脱氮,而且可实现有用细微粉尘即稀有金属的回收。此类装置还可应用于矿山、化工和建材等领域中的湿法除尘。     

A new design of groundwater sampling device and its application

Compounds in the atmosphere contaminate samples of groundwater. An inexpensive and simple method for collecting groundwater samples is developed to prevent contamination when the background concentration of contaminants is high. This new design of groundwater sampling device involves a glass sampling bottle with a Teflon-lined valve at each end. A cleaned and dried sampling bottle was connected to a low flow-rate peristaltic pump with Teflon tubing and was filled with water. No headspace volume was remained in the sampling bottle. The sample bottle was then packed in a PVC bag to prevent the target component from infiltrating into the water sample through the valves. In this study, groundwater was sampled at six wells using both the conventional method and the improved method. The analysis of trichlorofluoromethane（ CFC-11 ） concentrations at these six wells indicates that all the groundwater samples obtained by the conventional sampling method were contaminated by CFC-11 from the atmosphere. The improved sampling method greatly eliminated the problems of contamination, preservation and quantitative analysis of natural water.     

城市垃圾填埋场中废气测定方法

本文介绍了城市垃圾填埋场中的废气用注射器采样．经气相色谱热导池检测器测定的方法．该方法具有简单、快速、成本低、准确性高、精密度好等优点，由本方法测得的城市垃圾填埋场废气中甲烷和二氧化碳含量可作为设计沼气回收利用的可靠依据。     

陶瓷废水处理原理及常用固液分离方法比较

本文就陶瓷废水的产生来源及废水处理原理进行了分析，对佛山市该行业废水处理常用的固液分离方式进行了处理效果及技术经济比较，指出将常用于给水处理工艺的水力循环澄清池应用在陶瓷废水处理工艺中，与其它分离方法相比，不仅占地面积小，效率高，而且易于操作和控制，可实现废水的全部回用，并建议对这种高悬浮物、高浊度水的混凝反应过程进行自动控制以提高水处理的稳定性。     

大气自动监测系统在炼油厂的应用

运用日本引进的大气自动测定仪组成炼油厂的大气环境自动监测系统。运行结果表明，该系统自动化程度高，故障率低，操作简便，数据齐全，它的建立使我厂的大气环境监测上了一个新台阶．     

上海港散装液态危险品运输和监管现状

简要介绍了上海港散装液态危险货物运输开展的历史及迄今有关方面的现状，进而对上海港监为确保危险品散化运输在安全、防污、环保、贸易等之间的相互协调发展所采取的一系列相关措施加以概括、归纳，使之条理化。