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181.
气相色谱法测定工业废水中联苯与菲 总被引:3,自引:0,他引:3
文章研究了一种新的测定废水中联苯及菲含量的方法,该方法采用气相色谱薄涂柱,对联苯与菲进行了有效的分离与测定。该方法具有固定液用量少,柱温低,分离效果好,分析速度快等特点,利用该对废水样进行了测定,取得了满意的结果。 相似文献
182.
In this study, the surface chemical functional groups of Bacillus cereus biomass were identified by Fourier transform infrared (FTIR) analytical technique. It had been shown that the B. cereus cells mainly contained carboxyl, hydroxyl, phosphate, amino and amide functional groups. The potentiometric titration was conducted to explain the surface acid-base properties of aqueous B. cereus biomass. The computer program FITEQL 4.0 was used to perform the model calculations. The optimization results indicated that three sitesthree pKas model, which assumed the cell surface to have three distinct types of surface organic functional groups based on the IR analysis results, simulated the experimental results very well. Moreover, batch adsorption experiments were performed to investigate biosorption behavior of Cu(Ⅱ) and Pb(Ⅱ) ions onto the biomass. Obviously, the adsorption equilibrium data for the two ions were reasonably described by typical Langmuir isotherm. 相似文献
183.
Sardini P Robinet JC Siitari-Kauppi M Delay F Hellmuth KH 《Journal of contaminant hydrology》2007,93(1-4):21-37
An out-diffusion laboratory experiment using a non-reactive tracer was fitted using the Time Domain Diffusion (TDD) method. This rapid particle tracking method allows simulation of the heterogeneous diffusion based on pore-scale images and local values of diffusivities. The superimposed porosity and mineral 2D maps act as computation grids to condition diffusion pathways. We focused on a Palmottu granite sample, in which the connected pore space has a composite microstructure with cracks linking microporous minerals and is above the percolation threshold. Three main results were achieved: (i) When compared to the fitting obtained with one coefficient (best mean square residual R = 1.6 x 10(-2)), diffusion is shown to be suitably characterised with two coefficients related to cracks and microporous minerals (best R = 6.5 x 10(-4)), (ii) rather than imposing a local apparent diffusion coefficient D(a) independent of the local porosity Phi, a best fit is obtained by applying Archie's relationship D(a) = D(0) x G with G = Phi(m) to each pixel of the calculation grids (G is the geometry factor, D(0) is the diffusion coefficient in free fluid, and m is Archie's exponent), and (iii) the order of magnitude of the fitted diffusion coefficient or Archie's exponents (m=0 for microcracks and m=1.82 for microporous minerals) is physically realistic. 相似文献
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苏南地区新近沉积土的动剪切模量比与阻尼比--试验研究 总被引:3,自引:0,他引:3
苏南地区的场地土主要为漫滩相、湖沼相或冲湖相新近沉积软弱土,结构松散,沉积零乱,成分复杂,饱水可液化粉细砂层及粉土层较为发育,在地震或动力荷载的作用下有可能发生软土震陷或砂土液化。通过对苏南地区淤泥质粉质粘土、粘土、粉质粘土、粉质粘土与粉细砂互层土、粉土、粉砂、细砂和中粗砂等8类新近沉积土155个原状土样历时4年的试验研究,给出了该地区上述8类新近沉积土的动剪切模量比G/Gmax和阻尼比D随剪应变幅值γ变化的平均拟合曲线及其参数的推荐值。为便于一般工程应用,给出了这8类新近沉积土的G/Gmax-γ,和D—γ关系曲线的推荐值及其标准差。 相似文献
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钢管混凝土柱耐火性能和抗火设计的特点 总被引:5,自引:0,他引:5
简要论述了按ISO-834和GS9978-88规定的标准升温曲线升温作用下钢管混凝土柱耐火性能的特点,分析了影响钢管混凝土柱耐火极限的因素,说明了由于钢管和混凝土的共同工作且核心混凝土具有较好的吸热性能,从而使钢管混凝土柱具有较好的耐火性能。在进行钢管钢混凝土柱的抗火设计时,柱子外围只需进行适当的防火涂料保护,即可达到《高层用民建筑设计防火规范(GB50045-95)》对柱结构所要求的耐火极限。《高层用民建筑设计防火规范(GB50045-95)》中对钢结构柱防火保护层厚度的确定方法不适合于钢管混凝土。 相似文献
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Zisheng Xing Charles P.-A. Bourque Fan-Rui Meng Roger M. Cox D. Edwin Swift Tianshan Zha Lien Chow 《Ecological modelling》2008
In this paper we present a simple hybrid gap-filling model (GFM) designed with a minimum number of parameters necessary to capture the ecological processes important for filling medium-to-large gaps in Flux data. As the model is process-based, the model has potential to be used in filling large gaps exhibiting a broad range of micro-meteorological and site conditions. The GFM performance was evaluated using “Punch hole” and extrapolation experiments based on data collected in west-central New Brunswick. These experiments indicated that the GFM is able to provide acceptable results (r2 > 0.80) when >500 data points are used in model parameterization. The GFM was shown to address daytime evolution of NEP reasonably well for a wide range of weather and site conditions. An analysis of residuals indicated that for the most part no obvious trends were evident; although a slight bias was detected in NEP with soil temperature. To explore the portability of the GFM across ecosystem types, a transcontinental validation was conducted using NEP and ancillary data from seven ecosystems along a north-south transect (i.e., temperature–moisture gradient) from northern Europe (Finland) to the Middle East (Israel). The GFM was shown to explain over 75% of the variability in NEP measured at most ecosystems, which strongly suggests that the GFM maybe successfully applied to forest ecosystems outside Canada. 相似文献