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Acid-basecharacterizationoffoursulfidemineralsLinYuhuan(ResearchCenterforEco-EnvironmentaiSciences,ChineseAcademyofSciences,B... 相似文献
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对聚合铝溶液中总铝的测定方法提出改进,并利用t检验比较了改进方法和国家标准方法的测定结果。结果表明.准确控制EDTA的浓度和体积,可以省略杂质金属离子的掩蔽、解蔽和反滴的过程,改进方法和国家标准方法的结果无显著性差异。 相似文献
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EDTA滴定法测是水中的总硬度具有仪器价廉、步骤简单、操作方便、准确可靠等特点 ,是环境监测中通常采用的方法。通过大量的实验 ,对具体操作中有关问题进行探讨 ,发现了实验过程中有几方面需引起注意 ,并对数据准确可靠具有一定的保证 相似文献
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Fanhao Song Fengchang Wu Weiying Feng Zhi Tang John P. Giesy Fei Guo Di Shi Xiaofei Liu Ning Qin Baoshan Xing Yingchen Bai 《环境科学学报(英文版)》2018,30(12):116-125
Structural characteristics and proton binding properties of sub-fractions (FA3–FA13) of fulvic acid (FA), eluted stepwise by pyrophosphate buffer were examined by use of fluorescence titration combined with fluorescence regional integration (FRI) and differential fluorescence spectroscopy (DFS). Humic-like (H-L) and fulvic-like (F-L) materials, which accounted for more than 80% of fluorescence response, were dominant in five sub-fractions of FA. Based on FRI analysis, except the response of F-L materials in FA9 and FA13, maximum changes in percent fluorescence response were less than 10% as pH was increased from 2.5 to 11.5. Contents of carboxylic and phenolic groups were compared for fluorescence peaks of FA sub-fractions based on pH-dependent fluorescence derived from DFS. Static quenching was the dominant mechanism for binding of protons by FA sub-fractions. Dissociation constants (pKa) were calculated by use of results of DFS and the modified Stern-Volmer relationship. The pKa of H-L, F-L, tryptophan-like and tyrosine-like materials of FA sub-fractions exhibited ranges of 3.17–4.06, 3.12–3.97, 4.14–4.45 and 4.25–4.76, respectively, for acidic pHs. At basic pHs, values of pKa for corresponding materials were in ranges of 9.71–10.24, 9.62–10.99, 9.67–10.31 and 9.33–10.28, respectively. At acidic pH, protein-like (P-L) materials had greater affinities for protons than did either H-L or F-L materials. The di-carboxylic and phenolic groups were likely predominant sites of protonation for both H-L and F-L materials at both acidic and basic pHs. Amino acid groups were significant factors during proton binding to protein-like materials of FA sub-fractions at basic pH. 相似文献
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高锰酸盐指数是一个相对的条件性指标,其测定结果与溶液的酸度、高锰酸盐的浓度、加热温度和时间等有关。因此,测定时必须严格遵守操作规定,使其结果具有可比性。 相似文献
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