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471.
McCarthy K 《Environmental monitoring and assessment》2006,118(1-3):293-318
Semipermeable membrane devices (SPMDs) were deployed at eight sites within the Buffalo Slough, near Portland, Oregon, to (1)
measure the spatial and seasonal distribution of dissolved polycyclic aromatic hydrocarbon (PAH) and organochlorine (OC) compounds
in the slough, (2) assess the usefulness of SPMDs as a tool for investigating and monitoring hydrophobic compounds throughout
the Columbia Slough system, and (3) evaluate the utility of SPMDs as a tool for measuring the long-term effects of watershed
improvement activities. Data from the SPMDs revealed clear spatial and seasonal differences in water quality within the slough
and indicate that for hydrophobic compounds, this time-integrated passive-sampling technique is a useful tool for long-term
watershed monitoring. In addition, the data suggest that a spiking rate of 2–5 μg/SPMD of permeability/performance reference compounds, including at least one compound that is not susceptible to photodegradation,
may be optimum for the conditions encountered here. 相似文献
472.
苏玛罐采样-GC-FID/MS同时测定环境空气中多种VOCs 总被引:2,自引:0,他引:2
采用苏玛罐采样-大气预浓缩仪结合气相冷柱箱与Deans Switch中心切割技术,将C2~C3组分切割至HP-PLOT/Q+PT柱,用FID检测器分析,其余组分通过DB-1柱子分离后进入质谱分析,实现1次进样同时测定环境空气中57种PAMS和65种TO-15.结果表明:108种VOCs在0.15 nmol/mol~8.... 相似文献
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Chlorovinylannes (Lewisites) were produced and handled during WW I and WW II as chemical warfare agents. Residues of these
cwa and their metabolites are still present today and continue to contaminate soil and water.
A gas Chromatographic method for the detection and determination of chlorovinylarsines (Lewisites) and their metabolites is
shown. Lewisite II and Lewisite III, but not Lewisite I and the metabolites of Lewisite I and Lewisite II can be detected
and determined using GC/ECD. After derivatization with thiols, the sum of Lewisite I or Lewisite II and their metabolites
are detected. With the proper selection of the thiol, matrix interferences can be eliminated because of the different retention
times of the derivatives. 相似文献
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