电解锰行业清洁生产评价指标体系修订建议

现行电解锰行业清洁生产评价指标体系和清洁生产标准在行业清洁生产审核、绩效评定以及推动行业清洁生产技术应用和研发等方面发挥了显著的作用。但随着行业技术的快速进步,这两套评价指标存在部分指标值落后,直接引导清洁生产水平提升的指标少及应用范围窄等问题。在评价指标体系修订过程中,应发挥Ⅰ级基准值的先导性和前瞻性作用,突出直接反映清洁生产工艺和装备、污染物产生量的指标,扩大清洁生产评价指标体系的适用范围,制定出实用性和可操作性强的评价指标体系,以此推动电解锰行业清洁生产水平提升。     

医疗废物消毒集中处理工程技术规范修订思路及实施建议

高温蒸汽、微波消毒、化学消毒3项医疗废物消毒集中处理工程技术规范发布实施以来,对引导和规范我国医疗废物消毒集中处理工程建设和运行发挥了有益作用。然而,随着行业发展和技术升级,尤其是新型冠状病毒肺炎疫情发生之后,医疗废物处置行业面临新的挑战和机遇,医疗废物消毒集中处理工程的建设和运行也亟需与之匹配。在此背景下,修订后的高温蒸汽、微波消毒、化学消毒3项医疗废物消毒集中处理工程技术规范于2021年4月发布实施。基于对技术规范实施情况和行业发展现状的梳理,分析了上述3项技术规范修订的必要性,阐释了3项技术规范在建设规模、消毒处理工艺要求、污染控制技术要求、消毒效果检测频率等方面的修订思路,并且针对3项技术规范的实施提出了明确适用情景、明确技术定位、明确法律效力的建议。本研究可为新时期医疗废物消毒集中处理工程的建设和运行提供参考。     

模具CAD标准件库与资源库系统的设计

此文分析了传统方法建立标准件库的缺陷与存在的问题,提出了用作者开发的专用信息描述语言描述几何构形信息的思路。并介绍了基于信息描述语言建立标准件库和资源库的途径。     

GB/T5750-2006标准比色列缓冲法测定pH值的改进

本文依据GB/T 5750-2006标准比色列缓冲溶液比色法测定生活饮用水中的pH值,结合我实验室的检测经验对国标中指示剂的配制等重要环节进行了补充,并采用标准缓冲溶液比色法和玻璃电极法同时对自来水、河水、井水及矿泉水的pH值进行了测定,相对偏差在0.2%~1.3%之间,结果满意。     

A new synthesis of tetrachlorofluorodibenzo‐p‐dioxin

Abstract

The 1,2,3,4‐tetrachloro‐7‐fluorodibenzo‐p‐dioxin has been synthesized via condensation of 4‐fluorocatechol and pentachloronitrobenzene. This compound could be used as an internal standard for the analysis of 2,3,7,8‐tetrachlorodibenzo‐p‐dioxin by Chromatographic methods.     

SA8000与OHSMS试行标准

简要介绍了 SA80 0 0 (社会责任标准 )和 OHSMS(职业安全卫生管理体系 )试行标准的内容和要求 ;分析了两个标准的联系和区别 ;论述了实施 OHSMS试行标准的作用 ;提出了加强我国安全生产管理的建议。     

Emissions from soil fumigation in two raised bed production systems tarped with low permeability films

Raised beds are used to produce some high-value annual fruit and vegetable crops such as strawberry in California (CA) and tomato in Florida (FL), USA. Pre-plant soil fumigation is an important tool to control soil-borne pests in the raised beds. However, fumigant emissions have detrimental environmental consequences. Field trials were conducted to evaluate emissions of 1,3-dichloropropene (1,3-D) and chloropicrin (CP) in two different production systems with raised beds covered by different tarps. In the CA trial, InLine (60.8% 1,3-D and 33.3% CP) was drip-applied at 340 kg ha⁻¹ to 5 cm deep in the beds (30 cm high and 107 cm wide) tarped with polyethylene (PE) or virtually impermeable film (VIF). In the FL trial, carbonated Telone C35 (63.4% 1,3-D and 34.7% CP) was shank-applied at 151 kg ha⁻¹ to 20 cm deep in the beds (22 cm high and 76 cm wide) tarped with totally impermeable film (TIF). Emissions from tarped beds relative to furrows were contrary between the two trials. For the CA trial, the emission was 47% of applied 1,3-D and 27% of applied CP from PE tarped beds and 31% of applied 1,3-D and 15% of applied CP from VIF tarped beds, while that from uncovered furrows was <0.4% for both chemicals in both fields. In the FL trial, only 0.1% 1,3-D was emitted from the TIF tarped beds, but 27% was measured from the uncovered furrows. Factors contributing to the differences in emissions were chiefly raised-bed configuration, tarp permeability, fumigant application method, soil properties, soil water content, and fumigant carbonation. The results indicate that strategies for emission reduction must consider the differences in agronomic production systems. Modifying raised bed configuration and fumigant application technique in coarse textured soils with TIF tarping can maximize fumigation efficiency and emission reduction.     

甲醇气体标准样品的研制

介绍了甲醇气体标准样品的制备和定值方法,考察采用重量法制备氮气中甲醇标准气体样品的重现性、标准气体的均匀性和稳定性.试验表明,甲醇气体标准样品在气瓶内均匀性良好,在12个月研制期间没有不稳定趋势.摩尔分数为149.2×10-6甲醇气体标准样品,扩展不确定度为3%,能够满足环境污染源废气中甲醇气体监测的要求.     

《水质 化学需氧量的测定 重铬酸盐法》新旧标准比较

比较了《水质化学需氧量的测定重铬酸钾法》新标准《HJ 828—2017》与旧标准《GB/T 11914—1988》的区别。相较旧标准,新标准主要对取样体积、硫酸汞加入方法和加入量、氯离子浓度粗判、方法检出限和检出下限、质量保证与质量控制等内容进行了修订。针对新标准中校核要求、方法检出限计算及平行双样质量控制方面存在的问题进行探讨。     

化学需氧量现有2种标准分析方法若干问题研究

《水质化学需氧量的测定重铬酸盐法》(HJ 828-2017)和《高氯废水化学需氧量的测定氯气校正法》(HJ/T70-2001)是测定水中CODCr现有有效的2种标准方法.针对这2种方法存在的问题,通过实验给出操作建议.指出,对高氯废水稀释后采用《HJ828-2017》方法测定水中CODCr时,稀释倍数太大或稀释后COD...