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71.
建立了在突发性水污染事故中定量分析水样中甲醇、丙酮、乙腈、N,N-二甲基甲酰胺和N,N-二甲基乙酰胺等5种极性有机物的实验室和现场应急监测分析方法。采用顶空-车载气相色谱质谱法用于现场快速定性定量分析;顶空-气相色谱法用于实验室准确定量分析。通过优化顶空及气相参数,在最佳实验条件下测得顶空-气相色谱质谱法中甲醇、丙酮、乙腈、N,N-二甲基甲酰胺、N,N-二甲基乙酰胺等5种化合物的检出限分别为1.0、0.06、0.5、10.0、15.0 mg/L,平行测定7次结果的相对标准偏差分别为2.1%~3.8%,加标回收率为69.4%~104%;顶空-气相色谱法灵敏度高于气相色谱质谱法,检出限分别为0.08、0.01、0.03、1.7、1.7 mg/L,平行测定7次结果的相对标准偏差分别为2.5%~4.1%,加标回收率为78.1%~116%。 相似文献
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73.
顶空气相色谱测定空气中甲醇和乙醇含量,方法简单、快速,无需使用有机试剂。本方法以蒸馏水吸收空气中甲醇和乙醇,顶空进样经DB-624毛细管柱分离,氢火焰离子化检测器检测,时间定性,峰面积定量,其甲醇加标回收率为96.7%~104.6%,乙醇加标回收率为94.7%~103.8%,当在采样体积为40L的条件下,甲醇和乙醇最低检出质量浓度均为0.11mg/m^3。实际操作证明,该法能满足工业废气和空气中的甲醇和乙醇的监测。 相似文献
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Considering the increased trend to use renewable energy to meet electrical energy demands, a reliable performance also should be adopted in transmitting the generated power through the stable transmission and subtransmission systems for which nowadays Flexible AC Transmission System (FACTS) controllers are used extensively. Transient stability is one of the most important issues in power system stability analysis. FACTS devices have confirmed their capabilities in various aspects in power networks. In this paper, to improve transient stability of power systems, a shunt connected FACTS devices have been introduced, i.e., Static VAR compensators (SVCs). The SVC has the most diversified branches among FACTS devices. The main aim of this work is to study and analyze the impact of eight branches of SVC on improvement of transient stability and to choose the best of them. Simulations are performed in MATLAB/SIMULINK environment. 相似文献
76.
以顶空气相色谱法直接测定聚苯乙烯食品包装材料固体试样中的苯,甲本、对二甲苯和苯乙烯,最小检出量为10-10^10g,回收率为97.6%-102.5%。该法基体干扰小、操作简便。 相似文献
77.
78.
Parviz Abdolmaleki Faezeh Ghanati Hassan Sahebjamei Amir Sabet Sarvestani 《The Environmentalist》2007,27(4):435-440
Bio-effects of static magnetic fields on cell growth and cell death have been investigated in suspension-cultured tobacco
cells as undifferentiated, embryonic plant cell model. The cells in their logarithmic growth phase were exposed to static
magnetic field with the magnitudes of 10 mT and 30 mT for 5 h/day. Exposure to static magnetic field ceased the growth and
caused an increase in cell death of exposed tobacco cells compared to those cells which were not treated with the field. Promotion
of cell death was accompanied by a harmonized increase in the activity of peroxidase and increase of lignifcation of cell
walls. 相似文献
79.
Kari Hiltunen Jukka V. SeppÄlÄ Merja ItÄvaara Mika HÄrkönen 《Journal of Polymers and the Environment》1997,5(3):167-173
The biodegradability of lactic acid based poly(ester-urethanes) was studied using the headspace test method, which was performed
at several elevated temperatures. The poly(ester-urethanes) were prepared using a straight two-step lactic acid polymerization
process. The lactic acid is first condensation polymerized to a low molecular weight hydroxyl-terminated telechelic prepolymer
and then the molecular weight is increased with a chain extender such as diisocyanate. In the biodegradation studies the effect
of different stereostructures (different amounts of D-units in the polymer chain), the length of ester units, and the effect
of crosslinking on the biodegradation rate were studied. The results indicate that poly(ester-urethanes) do not biodegrade
at 25‡C, but at elevated temperatures they biodegrade well. The different stereostructures and crosslinking have a strong
influence on the biodegradation rate. The length of ester units in the polymer chain also affects the biodegradation rate,
but much less than crosslinking and stereostructure. 相似文献
80.