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91.
92.
采用气相色谱-质谱法(GC-MS)研究了不同溶剂对有机氯农药测定的影响。结果表明,有机氯农药在不同溶剂中的GC-MS响应值是有差异的,但保留时间不变,且随着有机氯农药质量浓度的增加,这种溶剂效应对大部分有机氯农药的作用减弱。经分析溶剂的极性对有机氯农药测定有显著的影响。 相似文献
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SOUL CHUN JAEHOON LEE ROLAND GEYER DAVID C. WHITE 《Journal of environmental science and health. Part. B》2013,48(5):731-740
Extraction is an important procedure for samples that contain soil because other compounds in soil may affect analysis of estrogens. This study was conducted to evaluate three different extraction methods for 17β-estradiol in soil. Sand, bentonite, and organic-rich silt loam were spiked with 1 mg kg? 1 of 17β-estradiol as a model compound of estrogens. 17β-estradiol and its metabolites, estrone and estriol, were extracted using (i) a modified Bligh and Dyer extraction, (ii) a pressurized fluid extraction, and (iii) a diethyl ether extraction, and measured by liquid chromatography tandem mass spectrometry. There were significant differences in the extraction efficiency for 17β-estradiol among the extraction methods and the soils: the efficiencies ranged from 10% to 97%. Overall, the diethyl ether extraction method had the largest efficiency of 17β-estradiol with 45% and 57% for bentonite and silt loam, respectively. Transformation of 17β-estradiol to estrone and estriol in the different extraction methods was less than 3.6% during the extraction procedures. This study underlined the importance of sample preparation for estrogen analysis in soil samples. 相似文献
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Testes mass in megachiropteran bats varies in accordance with sperm competition theory 总被引:4,自引:0,他引:4
D. J. Hosken 《Behavioral ecology and sociobiology》1998,44(3):169-177
Sperm competition is a widespread phenomenon influencing a range of characters, including investment in gonadal tissue. Conspecific
proximity is one factor which can influence the risk of sperm competition and hence testicular investment, and decreased confidence
of paternity may be one cost of group living. Aspects of female biology may also influence spermatogenic investment and sperm
morphology. This study examines the associations between relative testes mass and roost-group size across 17 species of Megachiroptera.
Associations between breeding season duration and investment in spermatogenesis are also examined, as are associations between
female reproductive tract dimensions and testes mass and dimensions of spermatozoa across all bats. Relative testes mass was
significantly positively associated with roost-group size at a species level and after appropriate phylogenetic control (pairwise
comparisons and comparison of independent contrasts). There were no significant relationships between breeding season duration
and relative testes mass. Across all bats, neither testes mass nor sperm length were significantly related to dimensions of
the female tract. The results are discussed in the context of sperm competition.
Received: 7 January 1998 / Accepted after revision: 8 August 1998 相似文献
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确定岩体斜坡滑动面抗剪强度的动态反分析方法 总被引:2,自引:0,他引:2
滑动结构面的抗剪强度在岩体滑坡的稳定性计算中是最重要的参数,也是最难以确定的。基于岩体抗剪强度是多种因素影响下的随机变量这一认识前提下,本文以西柏坡“中共中央解放军总部”旧址滑坡为例提出了确定岩体斜坡滑动面抗剪强度的动态反分析方法,并对该方法获得的抗剪强度的实用性进行了分析。结果表明,反分析方法是获得岩体斜坡滑动面抗剪强度的最经济、合理的途径。 相似文献
100.
采用高速摄影技术,考察了液化四氟乙烷发生小孔泄漏时,其水平泄漏和垂直泄漏的初始云团演化行为、泄漏的质量流率、喷射速度和喷射角,并与理论计算公式进行了对比。结果表明:水平喷射两相云团尾部出现涡流,涡流大幅加快了云团向空气中扩散的速率;垂直喷射的两相云团在地面形成液池,液池大幅增加了液化气体向空气中蒸发的速率。水平泄漏试验的喷射角与容器内超压变化规律相似,泄放初期喷射角逐渐增大,经历一段平坦期,到泄放末期喷射角减小。水平泄漏和垂直泄漏的初始喷射速度分别为25 m/s和20 m/s,与理论值26.6 m/s基本吻合。水平泄漏的质量流率的试验值和理论值分别为0.0598 kg/s和0.0684 kg/s,垂直泄漏的分别为0.0472 kg/s和0.059 6 kg/s,结果对比基本吻合,推荐的泄漏质量流率和小孔喷射速度公式可以用于液化四氟乙烷小孔泄漏。 相似文献