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861.
862.
利用原子吸收分光光度计上的燃烧头稍改进原子化和气路就可测定汞。该法具有灵敏度高,精密度和准确度均较好,操作简单,基本上自动化等优点。 相似文献
863.
雨水中微量过氧化氢的间接原子吸收测定 总被引:6,自引:0,他引:6
通过过氧化氢与重铬酸钾的定量反应,用原子吸收测铬的方法达到测定过氧化氢的目的。试验表明,该法用于雨水中微量过氧化氢的测定,试验令人满意,且操作方便。 相似文献
864.
1 IntroductionOnaninternationalscale,thenatureofurbanairpollutionhaschangedsignificantlyoverthelast50years.Inthe1950sand1960s,themostimportantenvironmentalhealthissuesstemmedfromtheoccurrenceofurbansmogs,anatmosphericcocktailcharacterizedbyhighconcen… 相似文献
865.
IntroductionKenya○shighpopulationgrowthratehascreatedpressureonthehighpotentialareas.Thishasresultedinthemigrationofpeopletouncultivated“marginal”landswhichmakeupabout80%ofthecountryandarepredominantlyoflowagriculturalproductivity(Hornetz,1990).These… 相似文献
866.
通过对胀形成形进行仿真计算和实际测试分析,比较了不同润滑条件下的应变分布,确定了胀形成形时的静摩擦系数μ值,研究分析了摩擦系数和材料参数n、r值对胀形成形的影响。 相似文献
867.
868.
Edward F. PeltierSamuel M. Webb Jean-François Gaillard 《Advances in Environmental Research》2003,8(1):103-112
The fate and bioavailability of pollutant metals is important to the long-term health of freshwater wetland systems, particularly in areas with elevated background levels of trace metals. Precipitation of some authigenic mineral phases in wetland sediments can potentially limit metal bioavailability through sequestration in low-solubility compounds, such as metal sulfides. Zinc and Pb concentrations were analyzed in water, plant and sediment samples taken from a metal-contaminated wetland in Chicago, IL, USA in order to assess metal fate and bioavailability, while X-ray absorption spectroscopy (XAS) studies were conducted to determine zinc speciation in the wetland sediments. The results showed sequestration of metal into the pond sediments, most likely in iron precipitate phases. In surface sediments, re-release of Zn and Pb into pore waters was correlated with microbial iron reduction, while the presence of sulfide in anoxic pore waters corresponded to decreased dissolved concentrations of both elements. Analysis of extended X-ray absorption fine structure (EXAFS) data confirmed that sulfide compounds dominated zinc speciation throughout the sediment. Uptake of trace metals in Phragmites plants was limited primarily to plant roots, while concentrations of both Pb and Zn in aquatic vegetation were significantly elevated, representing a potential bioaccumulation hazard. 相似文献
869.
石墨矿原子吸收分光光度法测定样品中的砷含量具有简便、快速、试剂用量少、样品直接测定等优点,精密度1.8%,检出限0.003,均优于其他分析方法. 相似文献
870.
T. R. Nelson R. J. Gillies D. A. Powell M. C. Schrader D. K. Manchesters D. H. Pretorius 《黑龙江环境通报》1987,7(5):363-372
Human amniotic fluid (HAF) is a dynamic system whose characteristics depend on continuous interchanges between fetal and maternal circulations. HAF reflects not only the environment of the fetus but may also provide information about fetal development or pathology. The concentration of HAF constituents varies with gestational age and pathological states. The number of the compounds currently implicated in fetal developmental pathology are relatively few. Currently used assay methods are not adequate to totally explain or predict the complex biochemistry of the fetus. The purpose of this work was to investigate HAF with NMR spectroscopy. In the present study HAF was obtained from 47 women undergoing routine amniocentesis. Cells were separated for karyological analysis and the supernatant was acid-extracted, lyophilized and re-suspended in D20 resulting in a concentration increase over native fluid. 1H NMR spectra were obtained at 360 MHz and 60 MHz. Eighteen compounds including several amino acids, were identified using parallel reference and standard addition protocols. NMR spectroscopy detected compounds of known clinical importance including glucose, leucine, isoleucine, lactate and creatinine. In conclusion, we have demonstrated that a number of physiologically relevant compounds are readily observable in HAF using 1H NMR spectroscopy. This technique can currently provide valuable information regarding HAF composition and has the potential of being used in vivo in the future. 相似文献