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251.
Seyed Jamaleddin Shahtaheri Farhad Ghamari Farideh Golbabaei Abbas Rahimi-Froushani Mohsen Abdollahi 《International journal of occupational safety and ergonomics》2013,19(4):377-388
Factors affecting solid phase extraction (SPE) of trans,trans-muconic acid (ttMA), as a benzene biomarker, including sample pH, sample concentration, sample volume, sample flow rate, washing solvent, elution solvent, and type of sorbent were evaluated. Extracted samples were determined by HPLC-UV(highperformance liquid chromatography-ultraviolet). The analytical column was C18, UV wave length was 259 nm, and the mobile phase was H2O/methanol/acetic acid run at flow rate of 1 ml/min. A strong anion exchange silica cartridge was found successful in simplifying SPE. There was a significant difference between recoveries of ttMA when different factors were used (p < .001). An optimum recovery was obtained when sample pH was adjusted at 7. There was no significant difference when different sample concentrations were used (p > .05). The optimized method was then validated with 3 different pools of samples showing good reproducibility over 6 consecutive days and 6 within-day experiments. 相似文献
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应用信息扩散原理,通过扩散函数对不完备信息进行适当的信息膨胀,建立观测样本和风险概率分布的映射关系,构建了基于信息扩散的城市区域安全生产风险计算模型.并以某市新北区的安全生产风险作为研究对象,选取该区域2005-2010年各年度建筑施工事故、火灾事故、工矿商贸事故的死亡人数和地区亿元GDP死亡率作为该区域安全生产风险的... 相似文献
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Kohei Sakat Aya Sakaguchi Masaharu Tanimizu Yuichi Takaku Yuka Yokoyam Yoshio Takahashi 《环境科学学报(英文版)》2014,26(2):343-352
Sources of Pb pollution in the local atmosphere together with Pb species, major ions, and heavy metal concentrations in a size-fractionated aerosol sample from Higashi-Hiroshima(Japan) have been determined by X-ray absorption near-edge structure(XANES) spectroscopy, ion chromatography, and ICP-MS/AES, respectively. About 80% of total Pb was concentrated in fine aerosol particles. Lead species in the coarse aerosol particles were PbC2O4, 2PbCO3·Pb(OH)2, and Pb(NO3)2, whereas Pb species in the fine aerosol particles were PbC2O4, PbSO4, and Pb(NO3)2. Chemical speciation and abundance data suggested that the source of Pb in the fine aerosol particles was different from that of the coarse ones. The dominant sources of Pb in the fine aerosol particles were judged to be fly ash from a municipal solid waste incinerator and heavy oil combustion. For the coarse aerosol particles, road dust was considered to be the main Pb source. In addition to Pb species, elemental concentrations in the aerosols were also determined. The results suggested that Pb species in size-fractionated aerosols can be used to identify the origin of aerosol particles in the atmosphere as an alternative to Pb isotope ratio measurement. 相似文献
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生化需氧量是在规定条件下,微生物分解存在水中的某些可氧化物质,特别是有机物所进行的生物化学过程中消耗溶解氧的量。生化需氧量质控样品的测定是检验一个化验员合格与否的重要依据,对于验证环境监测结果的准确性、精密性起着关键作用。而质控样品的测定与日常污水样品的测定是两个不同的概念,为了使初学者对质控样品的测定有一个直观的了解,详细叙述了质控样品的测定全过程。通过大量实验数据的采集,从实际出发证明该方法可靠有效。 相似文献
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