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Simas Angélica Mores Rúbia Steffens Juliana Dallago Rogério Marcos Kunz Airton Michelon William Fongaro Gislaine Viancelli Aline 《Environmental Chemistry Letters》2019,17(1):495-499
Environmental Chemistry Letters - Swine production generates large volumes of wastewater, rich in organic matter, nutrients and pathogens. Electrodisinfection is used to remove organic matter and... 相似文献
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Krüger RL Dallago RM Filho Ido N Di Luccio M 《Environmental monitoring and assessment》2009,158(1-4):355-363
This work reports the screening and characterization of odor compounds in gaseous effluents generated during the production of poultry feather and viscera meal, the by-products of the poultry meat industry. Chemical analysis was carried out by solid phase microextraction in the headspace (HS-SPME) mode. Exhaust air of thermal processing of poultry feather and viscera were sampled online from a bench-scale digester, condensed, and collected in sampling flasks. Both volatile and semivolatile organic compounds present in the condensed gases were extracted under agitation at constant temperature. The extracts were analyzed with a gas chromatograph coupled to a mass spectrometric detector (GC/MSD). The identification of compounds was carried out by comparing the mass spectra obtained with those from the Wiley library and quantification was accomplished through authentic analytical standards. For the determination of the best extraction conditions and analysis, extraction fibers of different coatings and polarities were tested: divinylbenzene/carboxen/polydimethyilsiloxane (DVB/CAR/PDMS), carbowax/divinylbenzene (CW/DVB), and polydimethylsiloxane (PDMS) and chromatography columns of different polarities: DB-WAX (polar) and DB-5 (nonpolar). The best extraction conditions and analysis of the compounds of interest were obtained by the use of the SPME fiber with DVB/CAR/PDMS coating and analysis by GC/MSD with polar capillary column. Several carboxylic acids were identified, as well as mercaptans, amines, and aldehydes of great environmental importance. 相似文献
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Aguilar CP Peruzzolo M Di Luccio M Dallago RM Filho Ido N 《Environmental monitoring and assessment》2006,116(1-3):103-110
The main purpose of this work was the preliminary qualitative study of organic compounds in wastewaters of swine slaughterhouses.
The samples were collected in a local abattoir and submitted to Liquid-Liquid Extraction (LLE) and Solid-phase Extraction
(SPE) with XAD-4TM resin as stationary phase. The instrumental analysis was performed by Gas Chromatography with Mass Spectrometer Detector
(GC/MSD). The compounds present in the LLE and SPE extracts were identified by the GC/MSD library (Wiley). The results pointed
out that SPE and LLE can extract practically the same classes of compounds at the same amounts. LLE works well for the extraction
of polar organic compounds, with acidified samples, while SPE presents a better performance for the extraction of less polar
organic compounds. Aldehydes were main class of the compounds extracted by SPE and LLE and decenal was the major aldehyde
identified. Fatty alcohols and carboxylic acids were also identified but in minor proportions. 相似文献
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