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Silva FA Neves RC Quintero-Pinto LG Padilha CC Jorge SM Barros MM Pezzato LE Padilha PM 《Chemosphere》2007,68(8):1542-1547
This paper presents a simple, fast and sensitive method to determine selenium in samples of feces and of fish feed by graphite furnace atomic absorption spectrometry (GFAAS) through the direct introduction of slurries of the samples into the spectrometer's graphite tube. The limits of detection (LOD) and quantification (LOQ) calculated for 20 readings of the blank of the standard slurries (0.50% m/v of feces or feed devoid of selenium) were 0.31 microg l(-1) and 1.03 microg l(-1), respectively, for the standard feces slurries and 0.35 microg l(-1) and 1.16 microg l(-1), respectively, for the standard feed slurries. The proposed method was applied in studies of bioavailability of selenium in different fish feeds and the results proved consistent with that obtained from samples mineralized by acid digestion using the microwave oven. 相似文献
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Juliano Gonçalves Pereira Vanessa Mendonça Soares Fernanda Gil de Souza Leonardo Ereno Tadielo Emanoelli Aparecida Rodrigues dos Santos Mário Celso Sperotto Brum Andreia Henzel Eduarda Hallal Duval Fernando Rosado Spilki Wladimir Padilha da Silva 《Food and environmental virology》2018,10(4):365-372
The aim of this study was to investigate hepatitis A virus (HAV), hepatitis E (HEV), and rotavirus (RV) in fresh and processed meat traded on the border of Brazil with Argentina and Uruguay. In total, 159 samples of raw and processed foods of animal origin were collected in Paso de los Libres, Argentina (n?=?53 raw meat, n?=?24 processed meat) and Rivera, Uruguay (n?=?55 raw meat, n?=?18 processed meat), or were seized by the Brazilian International Agricultural Surveillance System—VIGIAGRO (Brazil–Argentina border) (n?=?8 raw meat, n?=?1 bush meat). All samples were tested for the presence of HAV, HEV, and RV genomes. HAV genes were detected in 18.23% of samples and RV genes in 23.89%. No HEV-positive samples were detected. HAV was also detected in two of the VIGIAGRO samples. Processed meats from Argentina and Uruguay had a higher rate of HAV and RV than raw meat (P?>?0.05). The median HAV in the Argentinian and Uruguayan samples was 6.9?×?104 and 3.5?×?103 copies/g, respectively. The presence of RV viral genes in raw meats from Argentina was significant, and this was not observed in processed meats. The presence of HAV and RV genes in a significant portion of products from Argentina and Uruguay is a potential source of human infection. This also indicates precarious conditions of acquisition, processing, and manipulation, which could be improved by improved regulation of food across borders. 相似文献
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An investigation was made on the adsorption and kinetics of photodegradation of potassium hydrogenphthalate in an aqueous suspension of TiO(2). Two models, Langmuir and Freundlich, were used to describe the adsorption process and the model proposed by Langmuir-Hinshelwood (L-H) was employed to describe the kinetics of the photodecomposition reactions of hydrogenphthalate. The results of the adsorptions were fitted to the models proposed by Langmuir and Freundlich. Adsorption was found to be a function of the temperature, with adsorption capacity increasing from 2.4 to 4.5 mg/g when the temperature rose from 20 to 30 degrees C. The kinetic model indicates that the rate constant, k, of the first order reaction, is high in the 10.0 to 100 mg/l interval, which is coherent with the low value of the adsorption constant, K. The results fitted to the L-H model led to an equation that, within the range of concentrations studied here, theoretically allows one to evaluate the photodegradation rate. 相似文献
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de Abreu Íthalo Barbosa Silva de Sousa Maria Helena da Silva Andressa Pereira de Araújo Padilha Carlos Eduardo Sales Aldo Torres da Silva Antonio Samuel Alves Dutra Emmanuel Damilano Menezes Rômulo Simões Cezar 《Journal of Material Cycles and Waste Management》2023,25(3):1309-1324
Journal of Material Cycles and Waste Management - The use of food waste (FW) for the production of biofuels and value-added compounds is growing worldwide. However, the significant chemical... 相似文献
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Piovesan Bruna Padilha Aline Costa Morais Maíra Chagas Botton Marcos Grützmacher Anderson Dionei Zotti Moisés João 《Environmental science and pollution research international》2020,27(34):42472-42480
Environmental Science and Pollution Research - The use of pesticides is considered one of the most important threats to pollinators, especially since they are widely used in agriculture for pest... 相似文献
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José Cavalcante Souza Vieira Camila Pereira Braga Grasieli de Oliveira Aline de Lima Leite João Vitor de Queiroz Bruna Cavecci Alis Correia Bittarello Marília Afonso Rabelo Buzalaf Luiz Fabricio Zara Pedro de Magalhães Padilha 《Environmental Chemistry Letters》2017,15(4):717-724
Bioaccumulative metals such as mercury are found in increasing amounts in fish and their consumers. In the region of the Madeira River, in the Brazilian Amazon, mercury (Hg) is a predominant contaminant in the aquatic ecosystem. There is therefore a need to find specific biomarkers of mercury toxicity in fish to monitor contaminations. Here, mercury-bound proteins were identified in the liver tissues of fishes Mylossoma duriventre and Brachyplatystoma rousseauxii. Mercury was quantified in liver tissue, pellets and protein spots by graphite furnace atomic absorption. Proteins were fractionated by two-dimensional polyacrylamide gel electrophoresis and identified by mass spectrometry with electrospray ionization. We identified nine proteins linked to mercury and that presented biomarker characteristics of mercury. Among the proteins identified, isoforms of parvalbumin, ubiquitin-40S ribosomal protein S27a, brain-specific angiogenesis inhibitor 1-associated protein 2-like protein 2 and betaine–homocysteine S-methyltransferase 1 are notable for having the molecular function of binding to metallic ions. 相似文献
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