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Matthew Bates Paolo Bruno Mariangela Caputi Maurizio Caselli Gianluigi de Gennaro Maria Tutino 《Atmospheric environment (Oxford, England : 1994)》2008,42(24):6144-6151
The technique of thermal desorption (TD)–GC/MS was evaluated for measuring airborne, 4–6 ring polycyclic aromatic hydrocarbons (PAHs) collected onto quartz filters. TD provides a more readily automated and sensitive alternative to traditional solvent extraction, decreasing the time/cost of analysis and reducing the risk of analyte loss or sample contamination. The developed method was successfully applied to the analysis of PAH standard solutions loaded on sorbent tubes packed with quartz wool and the graphitized carbon black sorbent Carbograph2. The optimized method showed high desorption efficiency over the whole range of target PAHs with good precision, linearity and sensitivity. The proposed method was verified on an urban dust Standard Reference Material (SRM 1649a); the experimentally determined concentrations agreed with the certified ranges (95% confidence limit) for all target compounds except benzo[a]anthracene, which fell just outside the narrow certified range. The desorption efficiency and the reproducibility of the method was evaluated by analysing pieces of real sample filters sampled from urban air for a period of 24 h. The results confirmed the homogeneity of the filter and showed high recovery efficiencies for all target PAHs. 相似文献
3.
Riebsame WE 《Disasters》1985,9(4):295-300
Three recent cases of climate extremes are studied to identify human impacts and response strategies and to identify common characteristics that may help illuminate the nature of climate hazards. The 1980 heat wave in the central United States, 1981 cold wave in Boston, Massachusetts, and recent flooding and lake level rise in northern Utah, illustrate several important aspects of climate hazards that separate them from the more traditional set of catastrophic events (e.g. tornadoes, hurricanes and earthquakes) usually dealt with by hazards research and management. Among those characteristics are an emphasis on health impacts rather than physical damage, accumulative effects rather than short shocks, a tendency for impacts to accrue to certain socio-economic classes, and relatively slow onset. The management and research implications of these hazard characteristics are explored. 相似文献
4.
根据铝型材挤压模具的服役条件,采用宏观与微观相结合的分析方法,分析现场挤压模具的失效形式、失效性质和失效原因,并提出了提高模具使用寿命的一些措施. 相似文献
5.
热解析气相色谱法测定土壤中苯系物 总被引:1,自引:0,他引:1
建立了用热解析气相色谱法测定土壤中苯系物的方法.采用保留时间定性,外标法定量.方法检出限分别为:苯1.8 μg·L-1、甲苯3.5 μg·L-1、乙苯7.0 μg·L-1、间二甲苯8.6 μg·L-1、对二甲苯8.6 μg·L-1、邻二甲苯9.8 μg·L-1、苯乙烯10.0 μg·L-1;加标回收率在79%~100%之间,相对标准偏差为1.5%~3.9%.方法操作简便,快速,灵敏度高,能适应现代化的应急监测. 相似文献
6.
洪坚 《安全.健康和环境》2003,3(6):8-9
通过对炼油厂油品罐区消防、安全设施进行分析和改进,消除其对罐区的危害;对油罐主体腐蚀及加热器泄漏进行深入分析并提出实用的改进措施;完善生产与安全双重控制系统,为油品罐区标准化改造创造条件。 相似文献
7.
城市污水厂污泥热干燥处理技术及其应用分析 总被引:26,自引:0,他引:26
提出采用热干燥处理技术进一步降低脱水泥饼的含水率,介绍了现行的污泥热干燥处理技术,并就该技术在污泥处理中的应用尤其是在焚烧预处理中的应用进行了分析。 相似文献
8.
《环境科学学报(英文版)》2023,35(4):222-233
Anaerobic digestion (AD) of swine manure (SM) commonly shows low biogas output and unsatisfactory economic performance. In this study, thermophilic AD (TAD, 50 ± 1 °C) was combined with thermal hydrolysis pretreatment (THP, 170 °C/10 bar), to investigate its potential for maximizing biogas yield, securing successful digestion and microbial diversity, as well as improving energy balance. Four lab-scale continuously stirred tank reactors were operated for 300 days and compared with each other, i.e., reactor 1 (raw SM fed in mesophilic AD: RSM-MAD), reactor 2 (THP-treated SM fed in MAD: TSM-MAD), reactor 3 (RSM-TAD), and reactor 4 (TSM-TAD). The results showed that THP was efficient to increase methane production of SM, TSM-TAD mode led to the highest methane yield (129.8 ± 40.5 mL-CH4/g-VS/day) among the tests (p < 0.05). Although TAD was more likely to induce free ammonia (> 700 mg/L) or volatile fatty acids (> 6000 mg/L) accumulation compared with MAD in start-up phase, TSM-TAD treatment mode behaved a sustainable digestion process in a long-term operation. For TSM-TAD scenario, higher Shannon–Weaver (3.873) and lower Simpson index (0.061) indicated this mode ensured and enlarged the diversity of bacteria communities. Phylum Bathyarchaeota was dominant (59.3%−90.0%) in archaea community, followed by Euryarchaeota in the four reactors. RSM-MAD treatment mode achieved the highest energy output (4.65 GJ/day), TSM-TAD was less effective (−17.38 GJ/day) due to increased energy demands. Thus improving the energetic efficiency of THP units is recommended for the development of TSM-TAD treatment mode. 相似文献
9.
城市户外热环境的舒适性研究 总被引:5,自引:0,他引:5
介绍了户外热环境舒适性评价的几种方法,提出了户外热环境舒适评价指标OTCD,指出了在室内OTCD能与PMV很好吻合,并且OTCD的各项参数便于测量。 相似文献
10.
城市草坪的生态热效益 总被引:6,自引:0,他引:6
分析了草坪的能量平衡机理以及与环境之间的热湿交换关系,说明了草坪对空气具有降温增湿作用。通过重庆市区一些草坪实测数据分析发现草坪日平衡温度与空气日平均温度相等,说明草坪与空气之间保持热量的生态平衡。 相似文献