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The performance of Ce-OMS-2 catalysts was improved by tuning the fill percentage in the hydrothermal synthesis process to increase the oxygen vacancy density. The Ce-OMS-2 samples were prepared with different fill percentages by means of a hydrothermal approach (i.e. 80%, 70%, 50% and 30%). Ce-OMS-2 with 80% fill percentage (Ce-OMS-2-80%) showed ozone conversion of 97%, and a lifetime experiment carried out for more than 20?days showed that the activity of the catalyst still remained satisfactorily high (91%). For Ce-OMS-2-80%, Mn ions in the framework as well as K ions in the tunnel sites were replaced by Ce4+, while for the others only Mn ions were replaced. O2-TPD and H2-TPR measurements proved that the Ce-OMS-2-80% catalyst possessed the greatest number of mobile surface oxygen species. XPS and XAFS showed that increasing the fill percentage can reduce the AOS of Mn and augment the amount of oxygen vacancies. The active sites, which accelerate the elimination of O3, can be enriched by increasing the oxygen vacancies. These findings indicate that increasing ozone removal can be achieved by tuning the fill percentage in the hydrothermal synthesis process. 相似文献
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Xiuzheng Zhuang Yanqin Huang Huacai Liu Hongyou Yuan Xiuli Yin Chuangzhi Wu 《环境科学学报(英文版)》2018,30(7):261-270
Sewage sludge (SS) and deinking sludge (DS) were used to comparatively study the hydrothermal dewatering of sludge with different components. For a better overview, an insight into the relationship between physicochemical properties and dewaterability of hydrothermal sludge was provided. Results found that not all kinds of sludge were suitably conditioned by hydrothermal treatment (HT) in term of the elevation of dewaterability. Higher hydrothermal temperature tended to enhance the dewaterability of SS rather than DS, which was supported by the variation of their physicochemical properties (including water distribution, bonding energy, extracellular polymeric substance (EPS), particles size, acid functional groups and zeta potential in this study). In addition, the changes in surface morphology suggested that the reverse effect of HT on sludge dewaterability was mainly due to their dewatering behavior. For SS, the destruction of EPS structure leaded to the release of bound water, thereby strengthening sludge dewatering. Conversely, “Bridging effect” generated by lignocellulose in DS was beneficial for sludge dewatering; however, the increasing hydrothermal temperature degraded part of lignocellulose and weakened “bridging effect”, finally resulting in worse dewaterability of DS. 相似文献
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根据对医疗废物焚烧残余物中有毒有害物质的化验分析结果,确定焚烧残余物中有毒有害成分含量仍较高,部分指标超出标准值,必须对其进行稳定化/固化处理,避免对土壤及地下水环境造成污染.本文阐述了稳定化/固化处理原理及处理工艺,使医疗废物无害化、减量化和资源化的处理原则得以全面实现. 相似文献
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印刷线路板厂含铜污泥固化处理工艺研究 总被引:10,自引:0,他引:10
研究采用水泥作固化基材固化处理某印刷线路板厂酸性废水用石灰混凝所产生的含铜、锡、金的污泥 ,对固化块在不同 pH的水中重金属Cu2 +的浸出实验结果表明 :水泥固化处理该混凝污泥效果良好 ,控制合适的条件 ,可得到混合性能好、初凝时间适当、抗压强度较好的固化块。Cu2 +的浸出率低于允许浸出浓度。混凝过程中加入硫脲硅酸钠等助剂 ,可提高固化效果。研究还对几种不同配比的固化块抗压强度进行了探讨。 相似文献
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