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《中国环境监测》于2006年8月第22卷第4期发表了一篇名为“碱性高锰酸钾指数标准分析方法的错误”的文章,该文作者通过配制不同浓度的葡萄糖标准溶液,分别用酸性法与碱性法来测定其高锰酸盐指数值,对相应的结果与计算公式进行讨论,指出碱性高锰酸钾操作方法与计算公式均存在错误,并提出了碱性高锰酸钾测定的修正方法与公式。文章对上述观点和结论有不同的看法,从碱性高锰酸钾指数标准分析方法的试验操作步骤及方法原理的理解入手,进行相关的阐述和讨论。 相似文献
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用酸碱指示剂滴定法测定废水的中的OH-,CO3^2-,HCO3^-碱度时,S^2-对测定有干扰,此干扰可用H2O2掩蔽。 相似文献
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Takanori Hino Ryuichi Agawa Youichi Moriya Minoru Nishida Yasuhiro Tsugita Takao Araki 《Journal of Material Cycles and Waste Management》2009,11(1):42-54
Waste printed circuit boards contain valuable metals such as Au, Pd, Ag, and Cu that can be reutilized and harmful elements
such as Pb, Br, and Cr that must be removed from the viewpoint of environmental conservation. In this research, we examined
a method that separates the materials from printed circuit boards contained in discarded personal computers. After cutting
the printed circuit boards to a size of 20 × 20 mm, they were heated at 873 K under an Ar atmosphere to remove organic resins
containing elements such as C, H, and N. After heat treatment, the printed circuit boards were crushed using a planetary ball
mill and the pulverized powders were filtered. The fraction with a granularity of greater than 250 μm was separated into magnetic
and nonmagnetic materials by a magnetic field. Because the fraction with a granularity of less than 250 μm contained 39 mass%
of C, it was heated at 1273 K in an atmosphere of 95% Ar and 5% O2 to allow carbon combustion to take place, followed by metal reduction processing at the same temperature in an atmosphere
of 97% Ar and 3% H2. The basicity of the resulting powder was adjusted and the powder was heated at 1773 K under an Ar atmosphere. The proposed
method separated the slag and metal, and 80% of the valuable metals contained in printed circuit boards could be collected. 相似文献
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