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A new robust method for determination of hydrocarbons in water without use of Freon™ or other halogenated solvents has been validated and subjected to an interlaboratory exercise. The method is based on extraction with a light hydrocarbon (boiling point in the 39–69°C range), followed by cleanup for removal of polar components and detection by gas chromatography (GC) with flame ionisation (FID) detection. The performance characteristics of the method are comparable with that of the previous Freon-IR method with recoveries in the 60–80% range and reproducibility (between laboratory variations) of about 30%.
A screening method for hydrocarbons in the range 5 ppm and above based on infrared spectroscopy (IR), and a promising method for detection of low levels based on solid phase extraction (SPE) has been tested and validated. 相似文献
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Shanshan Zhao Zhu Tao Liwei Chen Muqiao Han Bin Zhao Xuelin Tian Liang Wang Fangang Meng 《Frontiers of Environmental Science & Engineering》2021,15(4):63
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《Journal of Manufacturing Processes》2014,16(3):405-413
Significant amount of work is reported on development of vegetable oil based metalworking fluids (MWFs). Many also report on development and performance evaluation of vegetable based oils. For many of these water-based MWFs with vegetable oils, much effort is focused on stable emulsification of vegetable oil in water using a variety of surfactants. It has been found that surfactant-free stable emulsification of oil in water is possible through ultrasonic vibration. However, emulsification through ultrasonic atomization has not yet been considered, and the feasibility of emulsified metalworking fluids through ultrasonic atomization has not been investigated. In this paper, stable emulsification of vegetable oil in water has been achieved through ultrasonic atomization without using any surfactant. The emulsified vegetable oil in water is directly used to investigate its effectiveness as MWF in milling operations. Lower cutting forces, chip thickness, and burr amount are observed with vegetable oil-in-water emulsion compared to conventional MWF. The experimental results show strong potential for vegetable oil-in-water emulsion obtained through ultrasonic atomization as an effective MWF. 相似文献
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