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还原-偶氮光度法测定废水中硝基苯的不确定度评估
引用本文:许伟,周俊,周晓惠,臧雯雯,胡佩.还原-偶氮光度法测定废水中硝基苯的不确定度评估[J].四川环境,2011,30(1):45-47.
作者姓名:许伟  周俊  周晓惠  臧雯雯  胡佩
作者单位:1. 江苏省东台市环境监测站,江苏东台,224200
2. 四川师范大学化学与材料学院,成都,610066
摘    要:以还原-偶氮光度法测定了废水中硝基苯的浓度,分析了测量过程中4个主要部分的不确定度。样品中硝基苯的浓度为0.500μg/mL,取包含因子k=2(95%置信概率),扩展不确定度为U=0.032μg/mL,结果可表示为:(0.500±0.032)μg/mL。此方法测定硝基苯的不确定度的评析,有利于更准确地表示测量结果。

关 键 词:不确定度  硝基苯  还原-偶氮光度法

Evaluating Uncertainty of Determining Nitrobenzene in Wastewater by Reduction Azo-photometry
XU Wei,ZHOU Jun,ZHOU Xiao-hui,ZANG Wen-wen,HU Pei.Evaluating Uncertainty of Determining Nitrobenzene in Wastewater by Reduction Azo-photometry[J].Sichuan Environment,2011,30(1):45-47.
Authors:XU Wei  ZHOU Jun  ZHOU Xiao-hui  ZANG Wen-wen  HU Pei
Institution:XU Wei1,ZHOU Jun1,ZHOU Xiao-hui1,ZANG Wen-wen1,HU Pei2(1.Dongtai Environmental Monitoring Station in Jiangsu Province,Dongtai,Jiangsu 224200,China,2.College of Chemistry & Materials Science,Sichuan Normal University,Chengdu 610066,China)
Abstract:Nitrobenzene concentration in wastewater was determined by reduction azo-photometry and the uncertainties of four primary parts of the determination process were analyzed.When the concentration of nitrobenzene was 0.500μg/mL and let the coverage factor k=2(confidence probability was 95%),the extended uncertainty U=0.032μg/mL.The result could be shown as Cnitrobenzene =(0.500±0.032)μg/mL.The uncertainty determined in this way could be more accurately.
Keywords:Uncertainty  nitrobenzene  reduction azo-hotometry  
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