| 丙酮－H_2O_2－ClO~－化学发光新体系的研究及应用 |
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| 引用本文： | 于振安,李焕.丙酮－H_2O_2－ClO~－化学发光新体系的研究及应用[J].环境保护科学,1996(2). |
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| 作者姓名： | 于振安 李焕 |
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| 作者单位： | 东北大学化学系 |
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| 摘 要： | 本文针对碘量法测定痕量次氯酸根（ＣｌＯ－）时，滴定中存在费时费试剂、痕量测定准确度欠佳的问题，研究并建立了流动注射化学发光法测定痕量ＣｌＯ－的新方法，具有较高的灵敏度、较好的准确度、重现性，为ＣｌＯ－的测定提供了一条新途径．该法在水质检验和环境监测中有一定的适用性．
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| 关 键 词： | 流动注射化学发光分析，丙酮，次氯酸根 |
THE STUDY AND APPLICATION OF ACETONE-H_2O_2-CLO￣-CHEMILUMINESCENCE SYSTEM |
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| Yu Zhenan,Li Huan.THE STUDY AND APPLICATION OF ACETONE-H_2O_2-CLO￣-CHEMILUMINESCENCE SYSTEM[J].Environmental Protection Science,1996(2). |
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| Authors: | Yu Zhenan Li Huan |
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| Abstract: | A new method is reported for the determination of trace amount of ClO-withacetone-H2O2-CLO-chemiluminescence system by FIA.The detection limit of the method is 4.9ng/ml for ClO-.If the range of CLO-concentration for the working curves was 3.0×10-8～3.0×10-ng/ml,the peak height was found to be linearly dependent on the concentration of CLO-.The relative standard deviation is less than 2.9%.The method was applied to determination ofClO- in water with satisfactory results. |
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| Keywords: | Flow Injection-chemiluminescence Analysis (FIA-C) Acetone Hypochorous Acid Group |
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