| 基于8—羟基喹啉与NO^—2—磺胺重氮盐的偶联反应示波极谱法测定NO^—2 |
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| 引用本文： | 刘海军,田亚赛.基于8—羟基喹啉与NO^—2—磺胺重氮盐的偶联反应示波极谱法测定NO^—2[J].干旱环境监测,1999,13(4):197-199. |
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| 作者姓名： | 刘海军 田亚赛 |
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| 作者单位： | 辽宁省本溪冶金高等专科学校!本溪117022 |
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| 摘 要： | 研究了８－羟基喹啉与ＮＯ＾－２－碘胺重氮盐偶联反应的条件及其产物的极谱行为。二阶导数波高与ＮＯ＾－２的浓度在０．００２－０．２ｍｇ／Ｌ内呈良好的线性关系，回收率为９８％－１０３％，已用于环境水样中ＮＯ＾－２的测定。
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| 关 键 词： | 羟基喹啉 示波极谱法 二氧化氮 磺胺重氮盐 |
DETERMINATION OF NO_2~- BY THE OSCILLOPOLAROGRAPHY WITH COUPLED ACTION OF 8-HYDROXYQUINOLINE AND THE DIAZONIUM SALT OF NO_2~-SULPHANILAMIDE |
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| Liu Haijun,Tian Yasai.DETERMINATION OF NO_2~- BY THE OSCILLOPOLAROGRAPHY WITH COUPLED ACTION OF 8-HYDROXYQUINOLINE AND THE DIAZONIUM SALT OF NO_2~-SULPHANILAMIDE[J].Arid Environmental Monitoring,1999,13(4):197-199. |
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| Authors: | Liu Haijun Tian Yasai |
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| Abstract: | The coupling reaction condition of 8-Hydroxyquinoline with NO\-2\+--Sulphanilamide diazotium salt and their polarographic behavior was studied.Linear relationship between secondary derivative wave height and concentration of NO\-2\+- can be obtained in the range of 0.002~0.2mg/l.The method has been applied to determing NO\-2\+- in environmental water with the recovery of 98~103%. |
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| Keywords: | NO\+-\-2 8-Hydroxyquinoline Oscillopolarography |
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