Evaluation of a precipitation collector for PCB analysis |
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| Affiliation: | 1. Division of Scientific Instrumentation & Management Center for Scientific Instrumentation, Korea Basic Science Institute, Chungbuk 28119, Republic of Korea;2. Department of Physics, Dankook University, Cheonan-si, Chungnam 31116, Republic of Korea;1. Université de Paris, Faculté de Santé, Paris, France;2. Inserm UMRS 1138, Team 17: Physiopathology of Ocular Diseases-Therapeutic Innovations, Centre de Recherche des Cordeliers, Paris, France;3. Sorbonne Université, UMR_S 1138, Centre de Recherche des Cordeliers, Paris, France;4. iCONICS Corefacility, ICM Institut du Cerveau et de la Moelle épinière, Hôpital de la Pitié-Salpêtrière, Paris, France;5. Department of Ophthalmology of University of Lausanne, Jules Gonin Hospital, Fondation Asile des Aveugles, Lausanne, Switzerland;6. Laboratoire de Pharmacologie-Toxicologie, Hôpital Maison Blanche, centre hospitalier et universitaire de Reims, Reims, France;7. AP-HP, Service d''Ophtalmologie, Hôpital Universitaire Necker-Enfants Malades, Paris, France;8. AP-HP, Service d''Endocrinologie, Gynécologie et Diabétologie Pédiatriques, Hôpital Universitaire Necker-Enfants Malades, Paris, France;9. Inserm U1016, Institut Cochin, Paris, France;10. Inserm UMR 1163, Institut Imagine, Université de Paris, Paris, France;11. AP-HP, Service de Néonatalogie, Hôpital Universitaire Necker-Enfants Malades, Paris, France;12. AP-HP, OphtalmoPôle, Hôpital Cochin, Paris, France;1. Flexible Electronic Devices and Sensors Lab, Department of Physics, New Jersey Institute of Technology, Newark, NJ 07102, USA;2. Department of Physics and Engineering Physics, Tulane University, New Orleans, LA 70118, USA |
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| Abstract: | The efficiency of a large wet-only precipitation collector for polychlorinated biphenyl (PCB) analysis was investigated using generator column-produced solutions. Total recoveries were quantitative for two experiments utilizing mixed Aroclor generator columns for the PCB source, with input-weighted average congener recoveries of 104 and 99%. Small losses were observed on the filter and collection reservoirs (> 3%), and no breakthrough to the second extraction cartridge was observed. Loss to the collector surface was 11 and 2%, and in the first case most likely reflects contamination rather than actual retention during the experiment. Individual congener recoveries generally rather than actual chlorination, a relationship that may be due mostly to analytical uncertainties for more highly chlorinated congeners. |
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