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水中毒死蜱的固相萃取气相色谱测定法
引用本文:胡鸿雁.水中毒死蜱的固相萃取气相色谱测定法[J].环境科学与技术,2008,31(8).
作者姓名:胡鸿雁
作者单位:国家城市供水水质监测网武汉监测站,湖北,武汉,430034
摘    要:建立水中毒死蜱的固相萃取——气相色谱FPD测定法。本方法的线性范围为0.25~5.00mg/L,回收率为94.2%,RSD为2.5%,检出限为0.25μg/L。该方法灵敏、准确,能很好地排除干扰,可满足水中痕量毒死蜱的测定。

关 键 词:  固相萃取  气相色谱  毒死蜱

Determination of Chlorpyrifos in Water by Solid-phase Extraction and Gas Chromatography
HU Hong-yan.Determination of Chlorpyrifos in Water by Solid-phase Extraction and Gas Chromatography[J].Environmental Science and Technology,2008,31(8).
Authors:HU Hong-yan
Abstract:An analytical method for determination of chlorpyrifos in water by solid-phase extraction(SPE) and GC-FPD was developed,with linear range of 0.25~5.00mg/L,recovery rate of 94.2%,relative standard deviation(RSD) 2.5%,detection limit 0.25μg/L.The method which is sensitive,accurate and able to eliminate the interference is suitable for determination of trace chlorpyrifos in water.
Keywords:water  solid-phase extraction  gas chromatography  chlorpyrifos
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