| 1-羟基芘的制备及其质谱光谱解析 |
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| 引用本文： | 马蒋赵. 1-羟基芘的制备及其质谱光谱解析[J]. 环境科学, 1992, 13(4): 27-30,8 |
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| 作者姓名： | 马蒋赵 |
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| 作者单位： | 北京市环境保护科学研究所 北京 |
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| 摘 要： | 报告了由芘制备1-羟基芘的方法,对所得产品进行了元素含量、质谱、核磁共振、紫外光谱、红外光谱和荧光光谱的分析。确定其组成为C_(6)H_(10)O_5,羟基在C_1位上;解析了质谱图中主要裂解产物的结构;给出特征光谱图,克分子消光(λ345nm)为3822.6。产品为较好的色谱纯品。
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| 关 键 词： | 1－羟基芘 芘 质谱 光谱 |
| 收稿时间： | 1991-12-05 |
Synthesis of 1-Hydroxypyrene and Its Identification |
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| Ma Jiangzhao. Synthesis of 1-Hydroxypyrene and Its Identification[J]. Chinese Journal of Environmental Science, 1992, 13(4): 27-30,8 |
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| Authors: | Ma Jiangzhao |
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| Affiliation: | Beijing Municipal Research Institute of Environmental Protection, Beijing 100037 |
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| Abstract: | A procedure for the preparation of 1-hydroxypyrene from pyrene was described. Its mass spectrum, nuclear magnetic resonance, infrared, ultraviolet and fluorescence spectra were determined. The results show that the compound thus prepared is a very pure product. |
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| Keywords: | 1-hydroxypyrene pyrene. |
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