| 绿色食品产地土壤中PAHs测定方法研究 |
| |
| 引用本文： | 毕鸿亮,饶勇,孙翠香,张浩原.绿色食品产地土壤中PAHs测定方法研究[J].生态环境,2007,16(2):467-470. |
| |
| 作者姓名： | 毕鸿亮 饶勇 孙翠香 张浩原 |
| |
| 作者单位： | 广东省生态环境与土壤研究所//广东省农业环境综合治理重点实验室,广东,广州,510650 |
| |
| 基金项目： | 广东省科学院优秀科技人才基金 |
| |
| 摘 要： | 对绿色食品产地土壤中多环芳烃的气相色谱质谱联用分析法进行了研究。样品经索氏提取后硅胶氧化铝复合柱净化,最后用GC/MS内标法进行定性定量分析。方法相关系数除苯并(a,h)蒽的相关系数R2=0.9970外,其余目标化合物的相关系数R2均大于0.9991,各化合物线性关系良好。方法加标回收率大多在70%至90%间,各目标化合物的方法检测限为2.2～40ng/kg。
|
| 关 键 词： | 绿色食品产地 土壤 多环芳烃 |
| 文章编号： | 1672-2175（2007）02-0467-04 |
| 收稿时间： | 2007-01-08 |
| 修稿时间： | 2007年1月8日 |
Study on the determination for PAHs in soil in green food producing |
| |
| BI HongLiang,RAO Yong,SUN CuiXiang,ZHANG HaoYuan.Study on the determination for PAHs in soil in green food producing[J].Ecology and Environmnet,2007,16(2):467-470. |
| |
| Authors: | BI HongLiang RAO Yong SUN CuiXiang ZHANG HaoYuan |
| |
| Institution: | Guangdong Key Laboratory of Agricultural Environment Pllution Integrated Control//Cuangdong Institute of Eco-Enviroment and Soil Science, Gongzhou 510650, China |
| |
| Abstract: | This paper describes a method for the determination of polycyclic aromatic hydrocarbons (PAHs) in soil of green food producing area. After Soxhlet extraction using dichloromethane a clean up extracts through multiplayer silica gel and alumina gel column extraction was performed. Sample were finally analyzed by gas chromatography-mass spectrometry using an internal Hexamethylbenzene standard. This method has a good linearity all PAHs related coefficient R2>0.999 1 except dibenza,hanthracene related coefficient R2=0.997. The most of recoveries for PAHs ranged between 70% and 90%.The method detection limits for the 16 PAHs mixture between 2.2 and 40 ng kg-1. |
| |
| Keywords: | green food producing area soil polycyclic aromatic hydrocarbons (PAHs) |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
