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空气预浓缩气相色谱/质谱法测定南京环境空气中二硫化碳
引用本文:薛光璞,田锋,孙成. 空气预浓缩气相色谱/质谱法测定南京环境空气中二硫化碳[J]. 四川环境, 2007, 26(1): 43-45
作者姓名:薛光璞  田锋  孙成
作者单位:南京市环境监测中心站,南京,210013;南京大学环境学院污染控制与资源化研究国家实验室,南京,210093
摘    要:采用不锈钢采样罐采集全量空气样品,使用空气预浓缩冷冻的方法从空气样品中提取二硫化碳,经气相色谱/质谱仪测定,判断确定空气恶臭物质的种类和污染来源。方法的最低检测浓度为0.003mg/m3,能够满足中国(TJ36-79)居住区大气中有害物质二硫化碳的最高容许浓度0.04mg/m3(一次值)标准的测定要求。

关 键 词:空气预浓缩  气相色谱/质谱测定  二硫化碳  恶臭  空气环境
文章编号:1001-3644(2007)01-0043-03
收稿时间:2006-06-22
修稿时间:2006-06-22

Determination of Carbon Disulfide in Air Samples Collected in Nanjing by Using Canisters and GC/MS
XUE Guang-pu,TIAN Feng,SUN Cheng. Determination of Carbon Disulfide in Air Samples Collected in Nanjing by Using Canisters and GC/MS[J]. Sichuan Environment, 2007, 26(1): 43-45
Authors:XUE Guang-pu  TIAN Feng  SUN Cheng
Abstract:To trace source and identify substances of an offensive odor emitted in Nanjing city sometimes,carbon disulfide was determined by sampling ambient air with specially prepared canisters,and was analyzed by gas chromatography-mass spectrometer after extraction with pre-concentrator.The lowest concentration of the method was 0.003 mg/m~3,and it satisfied the detection(requirement) for 0.04 mg/m~3 which is the permitted concentration of carbon disulfide for ambient air standard of hazard substances in inhabitant area of China(TJ36-79).
Keywords:Air pre-concentration  GC/MS  carbon disulfide  offensive odor  ambient air
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