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甘氨酸母液脱色废活性炭的微波-Fenton试剂氧化法再生
引用本文:陶长元,武凯,邱调军,刘作华,范兴,杜军. 甘氨酸母液脱色废活性炭的微波-Fenton试剂氧化法再生[J]. 化工环保, 2012, 32(2): 168-172
作者姓名:陶长元  武凯  邱调军  刘作华  范兴  杜军
作者单位:重庆大学化学化工学院,重庆,400030
基金项目:重庆市天然气化工重大专项,国家自然科学基金资助项目
摘    要:采用微波-Fenton试剂氧化法对甘氨酸母液脱色过程中产生的废活性炭进行再生,考察了废活性炭再生率的影响因素,并用SEM对再生活性炭进行了表征.实验结果表明,在Fenton试剂中n(H2O2)∶n(Fe2+)为24∶1、H2O2的浓度为25 mmol/L、溶液pH为3、反应温度为55℃、反应时间为18 min、微波功率为600 W时,废活性炭的再生率可达到75.80%.

关 键 词:甘氨酸  母液  活性炭  微波  芬顿试剂  再生  固体废物

Regeneration of Used Activated Carbon in Decoloration of Glycine Mother Liquor by Microwave-Fenton Reagent Oxidation Process
Tao Changyuan , Wu Kai , Qiu Tiaojun , Liu Zuohua , Fan Xing , Du Jun. Regeneration of Used Activated Carbon in Decoloration of Glycine Mother Liquor by Microwave-Fenton Reagent Oxidation Process[J]. Environmental Protection of Chemical Industry, 2012, 32(2): 168-172
Authors:Tao Changyuan    Wu Kai    Qiu Tiaojun    Liu Zuohua    Fan Xing    Du Jun
Affiliation:(College of Chemistry and Chemical Engineering,Chongqing University,Chongqing 400030,China)
Abstract:The used activated carbon in decoloration of glycine mother liquor was regenerated by microwave-Fenton reagent oxidation process.The factors affecting the regeneration were studied and the regenerated activated carbon was characterized by SEM.The experimental results show that when n(H2O2)∶n(Fe2+) of the Fenton reagent is 24∶1,the H2O2concentration is 25 mmol/L,the solution pH is 3,the reaction temperature is 55 ℃,the reaction time is 18 min and the microwave power is 600 W,the regeneration rate of the used activated carbon can reach 75.80%.
Keywords:glycine  mother liquor  activated carbon  microwave  Fenton reagent  regeneration  solid waste
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