| 水中几种有机污染物的SPE-HPLC联用测定技术 |
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| 引用本文： | 熊飞,陈玲,马娜.水中几种有机污染物的SPE-HPLC联用测定技术[J].环境科学与技术,2002,25(5):17-19. |
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| 作者姓名： | 熊飞 陈玲 马娜 |
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| 作者单位： | 同济大学污染控制与资源化研究国家重点实验室,上海,200092 |
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| 基金项目： | 国家自然科学基金项目资助 (599780 33) |
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| 摘 要： | 酚类及硝基苯是水中一类重要的优先控制污染物。通过对固相萃取 (SPE)技术与高效液相色谱 (HPLC)联用技术的研究 ,得出对于含酚类及硝基苯的水样采用 2 0 0mg的键合硅胶C1 8柱在水样pH值为 3 .0和过柱水样为 40mL时可得到较好的萃取及测定结果 ,从而提出一种对水中酚类物质及硝基苯测定具有灵敏度高、准确性好的分析方法。
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| 关 键 词： | 固相萃取(SPE) 高效液相色谱法(HPLC) 检测限 |
| 文章编号： | 1003-6504(2002)05-0017-03 |
| 修稿时间： | 2001年12月31 |
Determination of Several Organics in Contaminated Water by SPE-HPLC |
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| XIONG Fei,CHEN Ling,MA Na.Determination of Several Organics in Contaminated Water by SPE-HPLC[J].Environmental Science and Technology,2002,25(5):17-19. |
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| Authors: | XIONG Fei CHEN Ling MA Na |
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| Abstract: | Phenols and benzenes are important kinds of first control contamination. In terms of the solid phase extraction and high performance liquid chromatogram associated using research, we conclude a sensitive and exact analysis method using for the water sample with phenols and benzenes. When the sample volume is 40ml and the pH is 3.0, the sample analysis result can fulfill demand after being extracted by 200mg C 18 extraction column. |
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| Keywords: | solid phase extraction (SPE) high performance liquid chromatogram(HPLC) detection limits |
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