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原子吸收法测定水中锰的质量控制指标研究
引用本文:彭刚华,左燕君,陈晓峰,姜凌霄,胡梅,马芳,夏新.原子吸收法测定水中锰的质量控制指标研究[J].云南环境科学,2012(2):105-107.
作者姓名:彭刚华  左燕君  陈晓峰  姜凌霄  胡梅  马芳  夏新
作者单位:[1]江西省环境监测站,江西南昌330029 [2]北京科技大学,北京100083 [3]中国环境监测总站,北京100012
基金项目:本文得到了环保行业公益性科研项目资助(200809140).
摘    要:通过全国17个省份69家实验室的监测数据分析,研究确定了原子吸收法测定水中锰的质量控制指标和重复性限、再现性限,建议控制值为:浓度在0。1~3mg/L范围内的标准样品,控制RSD≤4%,RSD≤10%,RD≤5%,RE≤±10%;浓度在0.01—25mg/L范围内的实际样品,控制RD≤7%;同时,建议加标回收率控制在90%~110%。

关 键 词:  原子吸收法  质量控制指标

The Research on Quality Control Index for Determining Manganese in Water by Atomic Absorption Spectrometry
PENG Gang - huaI,ZUO Yan - jun,JIANG Ling - xiao,HU Mei,MA Fang,',XIA Xin.The Research on Quality Control Index for Determining Manganese in Water by Atomic Absorption Spectrometry[J].Yunnan Environmental Science,2012(2):105-107.
Authors:PENG Gang - huaI  ZUO Yan - jun  JIANG Ling - xiao  HU Mei  MA Fang    XIA Xin
Institution:3 (1. Jiangxi Provincial Environmental Monitoring Station, Nanchang Jiangxi 330029 China)
Abstract:On the basis of a large number of monitoring data from 69 laboratories of 17 provinces, we analyzed and determined the quality control index, repeatability 'limit and reproducibility limit for determing the manganese in water by atomic absorption spectrometry. The control limit has been suggested as follows: for the standard sample with a concentration of 0. lmg/L -3mg/L, the control RSD ≤4%, the RSD≤10%, RD≤5%, RE≤± 10% ; for the standard sample with a concentration of 0. 01mg/L -25mg/L, control RD ≤7%. Meanwhile, the recovery rate was suggested to be between 90% and 110%.
Keywords:manganese  atomic absorption spectrometry  quality control index
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