| 土壤中十氯酮检测方法研究 |
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| 引用本文： | 孙翠香,高原雪,刘婷琳,黄德银,毕鸿亮.土壤中十氯酮检测方法研究[J].生态环境,2011,20(4):727-729. |
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| 作者姓名： | 孙翠香 高原雪 刘婷琳 黄德银 毕鸿亮 |
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| 作者单位： | 广东省生态环境与土壤研究所//广东省农业环境综合治理重点实验室,广东广州,510650 |
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| 基金项目： | 广东省自然科学基金项目，广东省科学院测试基金项目 |
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| 摘 要： | 十氯酮（kepone）是一种毒性较高持久性有机污染物（POPs）。目前对于土壤中十氯酮的检测较少。采用索氏提取-硅胶氧化铝层析柱净化法,GC-MS对土壤中的十氯酮进行测定,该方法线性良好（r〉0.9996）,检测限较低（〈0.14μg.kg-1）,回收率稳定（平均值为90.1%~95.8%）。是测定土壤中十氯酮的较好方法。
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| 关 键 词： | 十氯酮 土壤 GC-MS |
The research of a method for determination of kepone in soil |
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| SUN Cuixiang,GAO Yuanxue,LIU Tinglin,HUANG Deyin,BI Hongliang.The research of a method for determination of kepone in soil[J].Ecology and Environmnet,2011,20(4):727-729. |
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| Authors: | SUN Cuixiang GAO Yuanxue LIU Tinglin HUANG Deyin BI Hongliang |
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| Institution: | SUN Cuixiang,GAO Yuanxue,LIU Tinglin,HUANG Deyin,BI Hongliang* Guangdong Key Laboratory of Agricultural Environment Pollution Integrated Control// Guangdong Institute of Ecology and Environmental and Soil Sciences,Guangzhou 510650,China |
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| Abstract: | Kepone was a kind of POPs. However, there is not a standard method to determinate it in soil so far. We created a new method, i.e., extracted with Acetone by Soxhlet extraction method and purified using silicaaluminum oxide chromatography, then determined it with GC-MS. This method had a good linearity （r〉0.999 6）, lower detect limit （〈0.14 μtg.kg-1） and a stable recovery rate （average value was 90.1%-95.8%）. It is a suitable method to determinate kepone in soil. |
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| Keywords: | kepone soil GC-MS |
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