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石墨炉原子吸收法测定室内积尘中铅含量不确定度评定
引用本文:莫招育,陈志明,谢鸿,毛敬英,林华,魏艳红. 石墨炉原子吸收法测定室内积尘中铅含量不确定度评定[J]. 环境科学与管理, 2013, 0(3): 124-128
作者姓名:莫招育  陈志明  谢鸿  毛敬英  林华  魏艳红
作者单位:广西壮族自治区环境保护科学研究院,广西南宁530022
摘    要:通过采集南宁市居民室内积尘,采用石墨炉原子吸收法进行铅含量的测定,根据JJF1059—1999〈〈测量不确定度评定与表示》对影响测量结果的不确定度分量进行了量化的计算,结果表明影响铅含量测定不确定度的主要因素为试样制备和校准曲线绘制,在该样品铅含量测定中,室内积尘中铅含量为21.4mg/kg,其扩展不确定度±2.78ms/kg。

关 键 词:不确定度  室内积尘    石墨炉原子吸收法

Determination of Uncertainty for Lead Content in Indoor Dust by Graphite Furnace Atomic Absorption Method
Mo Zhaoyu,Chen Zhiming,Xie Hong,Mao Jingying,Lin Hua,Wei Yanhong. Determination of Uncertainty for Lead Content in Indoor Dust by Graphite Furnace Atomic Absorption Method[J]. Environmental Science and Management, 2013, 0(3): 124-128
Authors:Mo Zhaoyu  Chen Zhiming  Xie Hong  Mao Jingying  Lin Hua  Wei Yanhong
Affiliation:(Environmental Protection Research Institute of Guangxi, Nanning 530022, China)
Abstract:With resident indoor dust from Nanning City, this study adopts graphite furnace atomic absorption method to deter- mine lead content. According to JJF 1059 - 1999 "Evaluation and Expression of Uncertainty in Measurement", the uncertainty in component results were calculated quantitatively. The results show that the main factors influencing the uncertainty of lead content are the sample preparation and calibration curves plotting. In this study, the lead content in indoor dust is 21.4 mg/kg with ex- tended uncertainty of±2. 78 mg/kg.
Keywords:uncertainty  indoor dust  lead  graphite furnace atomic absorption method
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