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吹扫捕集-气相色谱/质谱法测定水中25种挥发性有机物研究
引用本文:李亮,郝峰,石艳菊,李娜.吹扫捕集-气相色谱/质谱法测定水中25种挥发性有机物研究[J].环境科学与管理,2013(5):124-128.
作者姓名:李亮  郝峰  石艳菊  李娜
作者单位:内蒙古自治区环境监测中心站,内蒙古呼和浩特010011
摘    要:建立了吹扫捕集与气相色谱/质谱联用测定水中25种挥发性有机物的分析方法。该方法的加标回收率在90%-119%之间,响应因子(RF)的相对标准偏差均小于20%,检出限在0.04μg/L-0.22μg/L之间。该方法具有简单、快速、准确、灵敏,无其他有机物的污染等优点,适用于地表水、地下水和饮用水中挥发性有机物的测定,结果令人满意。

关 键 词:吹扫捕集  气相色谱-质谱  挥发性有机物  水环境

Determination of 25 Kinds of Volatile Organic Compounds in Water by Purge and Trap in Combination with GC/MS
Li Liang,Hao Feng,Shi Yanju,Li Na.Determination of 25 Kinds of Volatile Organic Compounds in Water by Purge and Trap in Combination with GC/MS[J].Environmental Science and Management,2013(5):124-128.
Authors:Li Liang  Hao Feng  Shi Yanju  Li Na
Institution:(Inner Mongolia Environmental Monitoring Center Station, Hohhot 010011, China)
Abstract:This study established a method to determine 25 kinds of volatile organic compounds in water by purge and trap in combination with gas chromatography and mass spectrometry (C,C/MS). The recovery ratios of the method were 90% - 119%. RF RSD was less than 20%. Using this method, the range of the lowest detection limits for 25 kinds of VOCs was 0. 04 μg/L 0. 22 μg/L. The method is simple, quick, sensitive and accurate, bringing no contamination. It is applicable for the determina- tion of VOCs in environmental water, underground water and drinking water samples.
Keywords:purge and trap  gas chromatography and mass spectrometry  volatile organic compounds  environmental water
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