| 热裂解气相色谱法测定水体中残留敌百虫 |
| |
| 引用本文： | 李爽,杜伟,李守富.热裂解气相色谱法测定水体中残留敌百虫[J].环境科学与管理,2009,34(7):100-104,74. |
| |
| 作者姓名： | 李爽 杜伟 李守富 |
| |
| 作者单位： | 1. 黑龙江省环境保护科学研究院,黑龙江,哈尔滨,150056
2. 东宁县环境监测站,黑龙江,东宁,157200 |
| |
| 摘 要： | 实验通过对熟裂解气相色谱及气-质联用技术测定水体中敌百虫的探讨，研究了气相色谱进样口裂解产物的检测方法，并确定了气相色谱的主要分析条件（进样口280℃，DB-225毛细管色谱柱及FPD检测器）。水样前处理结合环境检测的要求和特点，采用正己烷净化，三氯化碳提取的方式，建立了一套简单、有效及节省成本的前处理方法。检测方法的回收率在85．5％～104．5％之间，精密度小于5．89％，线性相关系数为0．99877，检出限为0．002μg／mL，说明该方法准确可靠，符合测定要求。该方法是按照中国关于水环境检测分析方法要求建立的，适合自然水体及养殖用水环境中敌百虫残留量的检测。
|
| 关 键 词： | 敌百虫 气相色谱 热裂解 |
Determination of Trichlorfon Residues in Water by Pyrolysis Gas Chromatography |
| |
| Li Shuang,Du Wei,Li Shoufu.Determination of Trichlorfon Residues in Water by Pyrolysis Gas Chromatography[J].Environmental Science and Management,2009,34(7):100-104,74. |
| |
| Authors: | Li Shuang Du Wei Li Shoufu |
| |
| Institution: | 1.Heilongjiang Environmental Protection Research Institute;Harbin 150056;China;2.Dongning Environmental Monitoring Station;Dongning 157200;China |
| |
| Abstract: | A method for the determination of trichlorfon in water was established by Pyrolysis Gas Chromatography and GC-MS,and confirmed Gas Chromatographic primary Analysis conditions about inlet temperature,DB-225 capillary column and detector of FPD.According to requirement and characteristics of inspective entironment,the fatiness was removed by n-hexane in water,and the trichlorfon extracted by Chloroform.The extraction was concentrated for determination of GC.A sample preparation method was set up that was simp... |
| |
| Keywords: | trichlorfon gas chromatography pyrolysis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
