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环境监测中POPs分析的关键问题与对策
引用本文:石毓岷.环境监测中POPs分析的关键问题与对策[J].生态与农村环境学报,2010,26(2).
作者姓名:石毓岷
作者单位:美国空气技术环境实验室,亚利桑那,85040,美国
摘    要:系统介绍了采用EPA8081A与8082方法进行环境样品中持久性有机污染物(POPs)分析的关键问题与对策。包括POPs的气相色谱分析与验证双柱系统,DDT与异狄氏剂在进样系统中的分解及其处理方法,应用目测识别法、手型法与透明复印胶片法等经验方法快速定性多氯联苯(PCBs)、氯丹与毒杀芬等多峰化合物,影响外标法准确定量PCBs、氯丹与毒杀芬等多峰POPs的关键因素,以及质量控制要求。提出应根据中国POPs的环境污染特点,建立相应的POPs标样库与标准图谱库,为中国的POPs污染调查与环境监测提供技术支持。

关 键 词:持久性有机污染物(POPs)  多氯联苯(PCBs)  氯丹  毒杀芬  气相色谱分析  验证双柱系统  SW-846综合分析法  

Key Problems in Screening Analysis of Persistent Organic Pollutants (POPs) in Environmental Monitoring and Countermeasures
SHI Yu-min.Key Problems in Screening Analysis of Persistent Organic Pollutants (POPs) in Environmental Monitoring and Countermeasures[J].Journal of Ecology and Rural Environment,2010,26(2).
Authors:SHI Yu-min
Abstract:A systematic introduction is presented to key problems and their countermeasures in screening analysis of persistent organic pollutants (POPs) in environmental samples using EPA 8081A and EPA 8082 methods,covering the double-column system for gas chromatographic analysis and validation of POPs,decomposition of DDT and endrin in the sample injection system and its countermeasures,rapid identification of multi-peaked compounds,such as polychlorinated biphenyl (PCBs),chlordane and toxaphene with empirical meth...
Keywords:persistent organic pollutants  polychlorinated biphenyls  chlordane  toxaphene  gas chromatographic analysis  double-column system  SW-846 manual  
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