| 多元素分析器分析砷遇到的问题与方法改进 |
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| 引用本文： | 翟永越,丁允.多元素分析器分析砷遇到的问题与方法改进[J].环境科学与管理,2007,32(3):165-167. |
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| 作者姓名： | 翟永越 丁允 |
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| 作者单位： | 1. 高邮市环境监测站,江苏,高邮,225600
2. 高邮市环境保护局,江苏,高邮,225600 |
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| 摘 要： | 依据新银盐分光光度法的基本原理,使用多元素分析器准确测定水体中砷的含量会遇到一些问题,如砷标准使用液浓度,吸收液配制,U型管DMF混合液加入量,脱脂棉装入U型管松紧程度,反应水样酸度,反应/吸收装置的致密性和一致性以及使用玻璃器皿的洗涤等,如果这些操作步骤不当都会给测定结果带来一定的误差,为了尽量减少这些误差,分析者对该项目测定方法作了一些探讨和改进,收到了良好的成效.
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| 关 键 词： | 多元素分析器 砷 问题 改进 多元素 分析器 问题 方法改进 Apparatus Analytical Element Improve Method Problem 测定方法 项目 误差 测定结果 操作步骤 洗涤 玻璃器皿 一致性 致密性 吸收装置 |
| 文章编号： | 1673-1212（2007）03-0165-03 |
| 修稿时间： | 2006-12-27 |
The Arsenical Analysis Encounters Problem and Method Improve in the Diverse Element Analytical Apparatus |
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| Zhai Yongyue,Ding Yun.The Arsenical Analysis Encounters Problem and Method Improve in the Diverse Element Analytical Apparatus[J].Environmental Science and Management,2007,32(3):165-167. |
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| Authors: | Zhai Yongyue Ding Yun |
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| Institution: | 1. Gaoyou Environmental Monitoring Station, Gaoyou 225600, China; 2. Gaoyou Environmental Protection Bureau, Gaoyou 225600, China |
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| Abstract: | The text analyzes the encountering problem that the diverse element analytical apparatus accurately determine arsenical content in water on the basis of basic principle of New Silver Salt photometric determination, such as arsenic standard usage liquid density; absorbing liquid compounding; DMF admixture liquid affiliation measure in U type tube; absorbent cotton packing into U type tube to a loose and close extent; reaction water sample acidity ; respond - absorption equip with the consistency and usage glassware of rinse etc. , these operations step is not appropriate to will give the measurement the result brings the certain error margin, for reducing these error margins to the best, writer makes the some study and improve with the analytical method of item, it receives good result. |
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| Keywords: | the diverse element analyzes apparatus arsenic problem improving |
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