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石墨炉原子吸收光谱法测定海水中痕量铅
引用本文:赖春苗,陆建军.石墨炉原子吸收光谱法测定海水中痕量铅[J].中国环境监测,2008,24(6).
作者姓名:赖春苗  陆建军
作者单位:广西北海海洋环境监测中心站,广西,北海,536000
摘    要:研究了APDC-DDTC/CCI4体系石墨炉原子吸收法测定海水中痕量Pb.在最佳务件测定海水中痕量铅与标准方法有良好的相关性(R=0.9969),统计检验表明,置信度为95%时,两方法之间没有显著差异.本法RSD%=1.1,精密度略优于标准方法,操作简便,节省时间.应用于海水中铅的分析,取得了令人满意的结果.

关 键 词:石墨炉原子吸收光谱法  海水  萃取  反萃取  

Determinations of Trace Lead in Seawater by Graphite Furnace Atomic Absorption Spectrometry
LAI Chun-miao,et al.Determinations of Trace Lead in Seawater by Graphite Furnace Atomic Absorption Spectrometry[J].Environmental Monitoring in China,2008,24(6).
Authors:LAI Chun-miao  
Institution:LAI Chun-miao,et al(Guangxi Beihai Marine Environmental Monitoring Centre,Beihai 536000,China)
Abstract:In this paper,determination of trace Lead in seawater by graphite furnace atomic absorption spectrometry with APDC-DDTC/CCl_4 system was studied.Under the optimum condition the result of this method was in excellent agreement with that obtained by standard method(R=0.9969).As shown by the test of hypothesis,when the confident level was 95%,there was no significant difference between this method and standard one.The RSD% of this method was 1.1,which was better than that of standard method.In addition,the pro...
Keywords:GFAAS  Seawater  Extraction  Back-extraction  Lead  
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