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废弃线路板热解油中酚类物质的提取与分离
引用本文:陈学娟,陈少纯,罗一鸣,刘勇. 废弃线路板热解油中酚类物质的提取与分离[J]. 环境科学与技术, 2011, 34(1): 184-186. DOI: 10.3969/j.issn.1003-6504.2011.01.044
作者姓名:陈学娟  陈少纯  罗一鸣  刘勇
作者单位:1. 中南大学化学化工学院,湖南长沙 410083;广州有色金属研究院,广东广州 510651
2. 广州有色金属研究院.广东广州 510651
3. 中南大学化学化工学院,湖南长沙,410083
摘    要:将FR-4型废弃线路板热解,并对热解油中含量最多的组分-酚类物质进行分离提取.比较研究线路板热解油的分离提取方法,探索出"碱液处理-酸化-萃取-减压蒸馏"的新方法,对分离出的组分进行GCMS(气质联用)测试.结果显示运用该方法对FR-4型线路板的热解油进行提取分离,得到的总酚占热解油的62.0%,其中苯酚的最高纯度可达...

关 键 词:废弃线路板  热解油  酚类  提取  分离

Extraction and Separation of Pyrolytic Oil from Pyrolysis of Scrap PCB
CHEN Xue-juan,CHEN Shao-chun,LUO Yi-ming,LIU Yong. Extraction and Separation of Pyrolytic Oil from Pyrolysis of Scrap PCB[J]. Environmental Science and Technology, 2011, 34(1): 184-186. DOI: 10.3969/j.issn.1003-6504.2011.01.044
Authors:CHEN Xue-juan  CHEN Shao-chun  LUO Yi-ming  LIU Yong
Affiliation:CHEN Xue-juan1,2,CHEN Shao-chun2,LUO Yi-ming1,LIU Yong2(1.School of Chemistry and Chemical Engineering,Central South University,Changsha 410083,China,2.Guangzhou Research Institute of Non-ferrous Metals,Guangzhou 510651,China)
Abstract:A bench-scaled experiment was conducted to recycle oil from pyrolyzing waste printed circuit boards of FR-4 type.This paper presents an innovative alkali treatment-adidification-extraction-vacuum distillation method to extract and separate oil,as well as the characterization of the components in the pyrolytic oil using GC-MS,which shows total phenols account for 62.0% in the oil and the best purity obtained is as high as 96.51%.
Keywords:scrap printed circuit boards(PCB)  pyrolytic oil  penols  extraction  separation  
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