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中药川附子非金属元素分析
引用本文:卢竞,顾兴平,顾永祚.中药川附子非金属元素分析[J].四川环境,2004,23(1):50-53.
作者姓名:卢竞  顾兴平  顾永祚
作者单位:1. 成都市第三人民医院,四川,成都,610031
2. 四川大学化学学院,四川,成都,610064
摘    要:本文论述了川附子非金属元素的分析:用ICP—AES法测定S、P和Si;离子色谱法测定Cl、S、P;极谱法和HG—AFS法测定痕量砷;ICP—AES和荧光法测定硒;GB法测定氯、氟和碘。应用提出的方法弄清了川附子用传统工艺食盐-胆巴混合溶液炮制前后非金属元素的含量与浓度变化,从而为中药化学成分进一步研究增添新内容一非金属元素及检测方法。

关 键 词:附子  非金属  感耦等离子体发射光谱  离子色谱  国家标准
文章编号:1001-3644(2004)01-0050-04
修稿时间:2003年2月25日

An Analysis of Non-metal Elements in Aconitum Carmichali Debx from Sichuan Origin
LU Jing,GU Xing-ping,GU Yong-zuo.An Analysis of Non-metal Elements in Aconitum Carmichali Debx from Sichuan Origin[J].Sichuan Environment,2004,23(1):50-53.
Authors:LU Jing  GU Xing-ping  GU Yong-zuo
Institution:LU Jing~1,GU Xing-ping~1,GU Yong-zuo~2
Abstract:This paper discusses the analysis of non-metal elements by following ways:Determination of P,S and Si by ICP-AES;Determination of Cl,P and S by IC;Determination of trace As by polarograph and HG-AFS;Determination of Se by ICP-AES and fluorometry;Determination of F,Cl and I by GB.By applying the proposed methods before and after the preparation with the table salt-Danpa mixture (conventional technics),the content and concentration change to determination of non-metal elements contained in Fuzi from Sichuan origin have been clear,and thus increases a new content(non-metal elements and detecting method)for futher study of the chemical composition of Chinese herbal medicines.
Keywords:Aconitum Carmichali Debx  non-metal element  ICP-AES  IC  GB
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