| 超声波提取-GC/MS法测定生物体内硝基苯类化合物 |
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| 引用本文： | 张莉,周卫华,王兆群. 超声波提取-GC/MS法测定生物体内硝基苯类化合物[J]. 环境监测管理与技术, 2013, 25(5): 19-22 |
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| 作者姓名： | 张莉 周卫华 王兆群 |
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| 作者单位： | 淮安市环境监测中心站;淮安市环境监测中心站;淮安市环境监测中心站 |
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| 基金项目： | 2011年江苏省环境监测科研基金资助项目（1111） |
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| 摘 要： | 以洪泽湖中6种代表性生物为研究对象，采用超声波法提取样品中硝基苯类化合物，用凝胶色谱净化、浓缩，气相色谱／质谱联用法测定。该法与索氏提取法在同等试验条件下进行加标回收试验，前者回收率高且稳定，简便可行。方法检出限为0．008μg／g～0．030μg／g，平均加标回收率为76．5％～109％，重复测定3次的RSD为1．5％～13．0％。
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| 关 键 词： | 硝基苯类化合物 超声波提取 凝胶色谱 气相色谱 质谱联用法 生物体 |
Ultrasonic GC/MS Method for the Determination of Nitrobenzene Compounds in Biological Samples |
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| ZHANG Li,ZHOU Wei-hua,WANG Zhao-qun. Ultrasonic GC/MS Method for the Determination of Nitrobenzene Compounds in Biological Samples[J]. The Administration and Technique of Environmental Monitoring, 2013, 25(5): 19-22 |
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| Authors: | ZHANG Li ZHOU Wei-hua WANG Zhao-qun |
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| Affiliation: | ( Huai＇an Environmental Monitoring Central Station, Huai＇an, Jiangsu 223001, China) |
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| Abstract: | Six representative biological samples from Hongze Lake were selected as researching objects. Ni- trobenzene compounds in biological samples were extracted by ultrasonic extraction. Gel chromatography was ap- plied to cleanup and concentration and quantification was done by GC/MS. Compared with the recoveries of the ultrasonic method and soxhlet extraction method under the same experimental conditions, the former method showed better recoveries and more stable. The detection limits were 0. 008μg/g - 0. 030μg/g. The average spike recovery were from 76.5% to 109% , and the RSDs of three times repeated measurements were from 1.5% to 13.0%. |
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| Keywords: | Nitrobenzene compounds Ultrasound Gel chromatography GC/MS Biology |
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