| 两波长定域同步荧光光谱法快速测定苯并(a)芘的研究 |
| |
| 引用本文： | 姚渭溪,熊涛,崔文烜,徐晓白.两波长定域同步荧光光谱法快速测定苯并(a)芘的研究[J].环境科学,1992,13(2):73-76. |
| |
| 作者姓名： | 姚渭溪 熊涛 崔文烜 徐晓白 |
| |
| 作者单位： | 中国科学院生态环境研究中心，中国科学院生态环境研究中心，中国科学院生态环境研究中心，中国科学院生态环境研究中心 北京 100085，北京 100085 江西省化学工业研究所，北京 100085，北京 100085 |
| |
| 基金项目： | 国家“七五”科技攻关课题 |
| |
| 摘 要： | 本文提出了快速测定环境样品中强致癌物BaP的两波长定域同步荧光光谱法(SFDW),样品经有机溶剂超声提取后,可以不经过预分离而直接用于测定,该方法操作简单、快速、灵敏,分析一个样品的时间由原来的1小时缩短为几分钟。其检测限为10~(-10)g,定量的线性范围至少可达三个数量级,该方法直接检测BaP的结果和样品经过分离后,采用高效液相色谱法(HPLC)测定的结果相近,其相对误差小于±20％,易于实现仪器化。
|
| 关 键 词： | 苯并（a）芘 人体污染 监测 致癌物 |
| 收稿时间： | 1991/5/16 0:00:00 |
Rapid Determination of Eenzo (a) Pyrene with Synchronous Fluorimetrie Scanning in Defined Range of Dual-Wavelengths |
| |
| Weixi Yao,Tao Xiong,Wenxian Cui and Xiaobai Xu.Rapid Determination of Eenzo (a) Pyrene with Synchronous Fluorimetrie Scanning in Defined Range of Dual-Wavelengths[J].Chinese Journal of Environmental Science,1992,13(2):73-76. |
| |
| Authors: | Weixi Yao Tao Xiong Wenxian Cui and Xiaobai Xu |
| |
| Institution: | Research Center for Eco-Environmental Sciences, Chinese Academy od Sciences, Beijing;Research Center for Eco-Environmental Sciences, Chinese Academy od Sciences, Beijing;Research Center for Eco-Environmental Sciences, Chinese Academy od Sciences, Beijing;Research Center for Eco-Environmental Sciences, Chinese Academy od Sciences, Beijing |
| |
| Abstract: | A rapid method for the determination of Bap using the synchronous fluorescence spectroscopic scanning in defined range of dual wavelengths (SFDW) was developed. No preseparation for the samples under analysis is needed. The method proved to be simple, rapid and sensitive. The minimum detection limit of BaP is about 5×10-10g and the linear range is over three orders of magnitude, The average relative deviation is less than ±20%. The results obtained with this method are comparable with those obtained with high performance liquid chromatography (HPLC). |
| |
| Keywords: | synchronous fluorimetry Benzo (a) pyrene Carcinogens |
| 本文献已被 CNKI 维普 等数据库收录！ |
| 点击此处可从《环境科学》浏览原始摘要信息 |
| 点击此处可从《环境科学》下载免费的PDF全文 |
|
